NIST High Temp. Superconducting Materials (HTS) Database:

NIST Standard Reference Database 62

Last Update to Data Content: 1996

DOI: https://doi.org/10.18434/T4KP8J


Bibliographic Information

Title: Irreversibility Temperatures in c-Axis-Oriented Powders of YBa2Cu3O7, Bi2Sr2CaCu2O8, and Bi2Sr2Ca2Cu3O10
Author(s): Y. Xu, M. Suenaga, Y. Gao, J.E. Crow, and N.D. Spencer
Publication: Physical Review B Volume: 42 Issue: 13 Year: 1990 Page(s): 8756-8759
Editor(s): Not Available
Publisher: American Physical Society
Language: English
Notes: Not Available
Keywords: Material Specification, Irreversibility Field

Materials and Properties

Bi:2212; [Bi-Sr-Ca-Cu-O]
Bi:2223; [Bi-Sr-Ca-Cu-O]
Material Specification for Bi:2212; [Bi-Sr-Ca-Cu-O] Process: Solid State Reaction
Notes: The authors cite Y. Xu et al., Phys. Rev. B, Vol. 39, 6667 (1989), and summarize the procedure as follows. "... we made a series of measurements... for a set of c-axis-oriented powders... bulk sintered specimens of the desired compositions were prepared. For alignment of the c axis of the powders along the field direction, the specimens were crushed to an average powder size of (about) 10 µm and encapsulated in epoxy under a magnetic field of (8T = 80 kG)."
Formula: Bi2Sr2CaCu2O8
Informal Name: Bi:2212
Chemical Family: Bi-Sr-Ca-Cu-O
Chemical Class: Oxide
Structure Type: Polycrystalline
Manufacturer: In House
Commercial Name: In House
Production Date:
Lot Number:
Production Form:

Irreversibility Field for Bi:2212; [Bi-Sr-Ca-Cu-O]
Temperature (K) Irreversibility Field (T)
15.7 5.0
17.2 4.0
21.0 2.0
25.4 1.0
29.1 0.7
35.1 0.4
37.3 0.3
42.5 0.14
51.5 0.07
54.5 0.02
64.2 0.0
Measurement Method: SQUID magnetometer
"A commercial superconducting quantum interference device (SQUID) magnetometer was used for the measurements of magnetic properties. Initially, the specimen was cooled to (about) 5 K in zero field and then a chosen magnetic-field value was set in several incremental steps. The sample was then slowly warmed up to a temperature well above Tc(H) and then slowly field cooled. During a warm-up and cool-down cycle, the temperature was varied by 0.5-K steps for (about) 15-K spans below Tc(H) and near T (H). Between these regions the temperature was changed by 1 or 2 K per step. At each temperature, three measurements (three scans) were taken with a 2-cm scan length... the trace of magnetic moment separates below T (H) and two straight lines were drawn from the low-temperature side, and the intersection of these was defined as T (H)."

Cautions: Evaluated Data
Digitized data were obtained from Figure 2 of the paper.
Material Specification for Bi:2223; [Bi-Sr-Ca-Cu-O] Process: Solid State Reaction
Notes: The authors cite Y. Xu et al., Phys. Rev. B, Vol. 39, 6667 (1989), and summarize the procedure as follows. "... we made a series of measurements... for a set of c-axis-oriented powders... bulk sintered specimens of the desired compositions were prepared. For alignment of the c axis of the powders along the field direction, the specimens were crushed to an average powder size of (about) 10 µm and encapsulated in epoxy under a magnetic field of (8T = 80 kG)."
Formula: Bi2Sr2Ca2Cu3O10
Informal Name: Bi:2223
Chemical Family: Bi-Sr-Ca-Cu-O
Chemical Class: Oxide
Structure Type: Polycrystalline
Manufacturer: In House
Commercial Name: In House
Production Date:
Lot Number:
Production Form:

Irreversibility Field for Bi:2223; [Bi-Sr-Ca-Cu-O]
Temperature (K) Irreversibility Field (T)
25.4 5.0
26.1 4.0
28.4 3.0
31.3 2.0
40.3 1.0
47.8 0.5
60.4 0.2
70.9 0.1
Measurement Method: SQUID magnetometer
"A commercial superconducting quantum interference device (SQUID) magnetometer was used for the measurements of magnetic properties. Initially, the specimen was cooled to (about) 5 K in zero field and then a chosen magnetic-field value was set in several incremental steps. The sample was then slowly warmed up to a temperature well above Tc(H) and then slowly field cooled. During a warm-up and cool-down cycle, the temperature was varied by 0.5-K steps for (about) 15-K spans below Tc(H) and near T (H). Between these regions the temperature was changed by 1 or 2 K per step. At each temperature, three measurements (three scans) were taken with a 2-cm scan length... the trace of magnetic moment separates below T (H) and two straight lines were drawn from the low-temperature side, and the intersection of these was defined as T (H)."

Cautions: Evaluated Data
Digitized data were obtained from Figure 2 of the paper.