NIST High Temp. Superconducting Materials (HTS) Database:

NIST Standard Reference Database 62

Last Update to Data Content: 1996

DOI: https://doi.org/10.18434/T4KP8J


Bibliographic Information

Title: Fracture Toughness Measurements of YB2Cu3Ox Single Crystals
Author(s): R.F. Cook, T.R. Dinger, and D.R. Clarke
Publication: Applied Physics Letters Volume: 51 Issue: 6 Year: 1987 Page(s): 454-456
Editor(s): Not Available
Publisher: American Institute of Physics
Language: English
Notes: Not Available
Keywords: Material Specification, Hardness, Fracture Toughness

Materials and Properties

Y:123; [Y-Ba-Cu-O]
Material Specification for Y:123; [Y-Ba-Cu-O] Process: Solid State Reaction
Notes: "Single crystals... were prepared by a liquid-assisted growth process in which a cold-pressed pellet of off-stoichiometry YBa2Cu3Ox was fired under controlled atmosphere conditions... The crystals produced were tabular in morphology, approximately 400 µm square and 200 µm thick."
Formula: YBa2Cu3O7+x
Informal Name: Y:123
Chemical Family: Y-Ba-Cu-O
Chemical Class: Oxide
Structure Type: Single Crystal
Manufacturer: In House
Commercial Name: In House
Production Date:
Lot Number:
Production Form:

Hardness for Y:123; [Y-Ba-Cu-O]
Temperature (°C) Hardness (GPa)
296 8.7 ± 2.4
Measurement Method: Vickers indentation
"The crystals were first mounted in a thermoplastic wax on cylindrical stubs such that the basal plane was approximately perpendicular to the stub axis. The stubs were then clamped in the stage of a microindenter after aligning the basal plane perpendicular to the indenter loading direction. Indentations were made on the surface of the crystals with a Vickers diamond pyramid at contact loads between 0.1 N and 2 N for a peak-load contact time of 5 s. Indentations were made in ambient air. Most indentations were oriented with the diagonals of the square impression parallel to the [100] and [001] directions."

Cautions: Evaluated Data
Fracture Toughness for Y:123; [Y-Ba-Cu-O]
Temperature (K) Fracture Toughness (MPa·m1/2)
296 1.1 ± 0.3
Measurement Method: Vickers indentation
"The crystals were first mounted in a thermoplastic wax on cylindrical stubs such that the basal plane was approximately perpendicular to the stub axis. The stubs were then clamped in the stage of a microindenter after aligning the basal plane perpendicular to the indenter loading direction. Indentations were made on the surface of the crystals with a Vickers diamond pyramid at contact loads between 0.1 N and 2 N for a peak-load contact time of 5 s. Indentations were made in ambient air. Most indentations were oriented with the diagonals of the square impression parallel to the [100] and [001] directions."

Cautions: Evaluated Data