NIST High Temp. Superconducting Materials (HTS) Database:

NIST Standard Reference Database 62

Last Update to Data Content: 1996

DOI: https://doi.org/10.18434/T4KP8J


Bibliographic Information

Title: Elastic Behavior of a Y-Ba-Cu-O Sample Prepared by the MPMG Method
Author(s): R.R. Reddy, M. Murakami, S. Tanaka, and P.V. Reddy
Publication: Physica C Volume: 257 Issue: Not Available Year: 1996 Page(s): 137-142
Editor(s): Not Available
Publisher: Elsevier Science Publishers B.V.
Language: English
Notes: Not Available
Keywords: Material Specification, Density (mass), Debye Temperature, Elastic Modulus, Shear Modulus, Poisson's Ratio, Bulk Modulus, Sound Velocity

Materials and Properties

Y:123; [Y-Ba-Cu-O]
Material Specification for Y:123; [Y-Ba-Cu-O] Process: Melt Processed
Notes: The authors cite M. Murakami, Mod. Phys. Lett. B, Vol. 4, 163 (1990), and summarize the procedure as follows. "The YBa2Cu3Ox sample with (a mole fraction of 30 %) of Y2BaCuO5 inclusions was prepared by the MPMG process. In this method, the Y-Ba-Cu-O sample is first melted at temperatures above 1300 °C and cooled down to room temperature. Later it is reheated up to a temperature region between 1000-1200 °C followed by rapid cooling to a temperature at which the superconducting phase starts nucleating. During remelting Y2O3 reacts with the liquid to form Y2BaCuO5 which in turn reacts with the liquid to produce the YBa2Cu3O7 phase. As a result, fine Y211 particles of about 1 µm in diameter are dispersed in the matrix of 123 phase."
Formula: YBa2Cu3Ox·yY:211
Informal Name: Y:123
Chemical Family: Y-Ba-Cu-O
Chemical Class: Oxide
Structure Type: Polycrystalline
Manufacturer: In House
Commercial Name: In House
Production Date:
Lot Number:
Production Form:

Density (mass) for Y:123; [Y-Ba-Cu-O]
Temperature (K) Density (g cm-3)
295 5.952
Measurement Method: Archimedes' method
"The bulk density (was) determined by the Immersion technique..." No additional measurement details were noted.

Cautions: Unevaluated Data
Debye Temperature for Y:123; [Y-Ba-Cu-O]
Temperature (K) Debye Temperature (K)
295 379
Measurement Method: Ultrasonic method
The authors cite Y.V. Ramana et al., Acoustics Lett., Vol. 13, 85 (1988), and summarize the procedure as follows. "Ultrasonic longitudinal velocity measurements were carried out by the pulse transmission technique over a temperature range of 80-300 K on a sample with dimensions of 4 mm in thickness and 12 mm in diameter. X- and Y-cut PZT transducers with a fundamental frequency of 1 MHz were used for transmitting and receiving the longitudinal (V ) and shear (Vc) waves. The transit time of ultrasound has been measured up to an accuracy of 0.01 µs using a 100 MHz digital storage oscilloscope [Tektronix Model No. 2221]. ... The overall accuracy of the velocity measurements work out to be ±10 m/s."

Cautions: Evaluated Data
Elastic Modulus for Y:123; [Y-Ba-Cu-O]
Temperature (K) Elastic Modulus (GPa)
80 165
88 165
98 166
110 168
117 169
129 164
138 159
148 156
160 154
167 151
179 146
190 143
198 139
208 137
219 132
227 130
239 126
248 121
258 118
269 115
279 107
288 104
300 101
Measurement Method: Ultrasonic method
The authors cite Y.V. Ramana et al., Acoustics Lett., Vol. 13, 85 (1988), and summarize the procedure as follows. "Ultrasonic longitudinal velocity measurements were carried out by the pulse transmission technique over a temperature range of 80-300 K on a sample with dimensions of 4 mm in thickness and 12 mm in diameter. X- and Y-cut PZT transducers with a fundamental frequency of 1 MHz were used for transmitting and receiving the longitudinal (V ) and shear (Vc) waves. The transit time of ultrasound has been measured up to an accuracy of 0.01 µs using a 100 MHz digital storage oscilloscope [Tektronix Model No. 2221]. ... The overall accuracy of the velocity measurements work out to be ±10 m/s."

Cautions: Evaluated Data
"As the porosity of the samples is about 4%, the... elasticity parameters have been corrected to zero porosity..." Digitized data were obtained from Figure 2 of the paper.
Shear Modulus for Y:123; [Y-Ba-Cu-O]
Temperature (K) Shear Modulus (GPa)
295 45.4
Measurement Method: Ultrasonic method
The authors cite Y.V. Ramana et al., Acoustics Lett., Vol. 13, 85 (1988), and summarize the procedure as follows. "Ultrasonic longitudinal velocity measurements were carried out by the pulse transmission technique over a temperature range of 80-300 K on a sample with dimensions of 4 mm in thickness and 12 mm in diameter. X- and Y-cut PZT transducers with a fundamental frequency of 1 MHz were used for transmitting and receiving the longitudinal (V ) and shear (Vc) waves. The transit time of ultrasound has been measured up to an accuracy of 0.01 µs using a 100 MHz digital storage oscilloscope [Tektronix Model No. 2221]. ... The overall accuracy of the velocity measurements work out to be ±10 m/s."

Cautions: Evaluated Data
"As the porosity of the samples is about 4%, the... elasticity parameters have been corrected to zero porosity..."
Poisson's Ratio for Y:123; [Y-Ba-Cu-O]
Temperature (K) Poisson's Ratio (no unit)
295 0.14
Measurement Method: Ultrasonic method
The authors cite Y.V. Ramana et al., Acoustics Lett., Vol. 13, 85 (1988), and summarize the procedure as follows. "Ultrasonic longitudinal velocity measurements were carried out by the pulse transmission technique over a temperature range of 80-300 K on a sample with dimensions of 4 mm in thickness and 12 mm in diameter. X- and Y-cut PZT transducers with a fundamental frequency of 1 MHz were used for transmitting and receiving the longitudinal (V ) and shear (Vc) waves. The transit time of ultrasound has been measured up to an accuracy of 0.01 µs using a 100 MHz digital storage oscilloscope [Tektronix Model No. 2221]. ... The overall accuracy of the velocity measurements work out to be ±10 m/s."

Cautions: Evaluated Data
Bulk Modulus for Y:123; [Y-Ba-Cu-O]
Temperature (K) Bulk Modulus (GPa)
295 48.7
Measurement Method: Ultrasonic method
The authors cite Y.V. Ramana et al., Acoustics Lett., Vol. 13, 85 (1988), and summarize the procedure as follows. "Ultrasonic longitudinal velocity measurements were carried out by the pulse transmission technique over a temperature range of 80-300 K on a sample with dimensions of 4 mm in thickness and 12 mm in diameter. X- and Y-cut PZT transducers with a fundamental frequency of 1 MHz were used for transmitting and receiving the longitudinal (V ) and shear (Vc) waves. The transit time of ultrasound has been measured up to an accuracy of 0.01 µs using a 100 MHz digital storage oscilloscope [Tektronix Model No. 2221]. ... The overall accuracy of the velocity measurements work out to be ±10 m/s."

Cautions: Evaluated Data
"As the porosity of the samples is about 4%, the... elasticity parameters have been corrected to zero porosity..."
Sound Velocity for Y:123; [Y-Ba-Cu-O]
Mode () Temperature (K) Sound Velocity (km/s)
Longitudinal 295 4.120
Shear 295 2.650
Measurement Method: Ultrasonic method
The authors cite Y.V. Ramana et al., Acoustics Lett., Vol. 13, 85 (1988), and summarize the procedure as follows. "Ultrasonic longitudinal velocity measurements were carried out by the pulse transmission technique over a temperature range of 80-300 K on a sample with dimensions of 4 mm in thickness and 12 mm in diameter. X- and Y-cut PZT transducers with a fundamental frequency of 1 MHz were used for transmitting and receiving the longitudinal (V ) and shear (Vc) waves. The transit time of ultrasound has been measured up to an accuracy of 0.01 µs using a 100 MHz digital storage oscilloscope [Tektronix Model No. 2221]. ... The overall accuracy of the velocity measurements work out to be ±10 m/s."

Cautions: Evaluated Data