NIST High Temp. Superconducting Materials (HTS) Database:

NIST Standard Reference Database 62

Last Update to Data Content: 1996

DOI: https://doi.org/10.18434/T4KP8J


Bibliographic Information

Title: C-axis Thermal Expansion of the Tl2Ba2CaCu2Ox Superconductor
Author(s): E.F. Skelton, W.T. Elam, M.S. Osofsky, P. Lubitz, M.Z. Harford, and A.K. Singh
Publication: Physical Review B Volume: 39 Issue: 4 Year: 1989 Page(s): 2779-2780
Editor(s): Not Available
Publisher: American Physical Society
Language: English
Notes: Not Available
Keywords: Material Specification, Thermal Expansion

Materials and Properties

Tl:2212; [Tl-Ba-Ca-Cu-O]
Material Specification for Tl:2212; [Tl-Ba-Ca-Cu-O] Process: Sputtering
Notes: "Thin Films of Tl2Ba2CaCu20x were prepared by evaporating a bulk sample of same composition in vacuum with an electron beam. The reactants were deposited on a polished (100) face of an MgO single crystal maintained at 300 °C. The films were then annealed in air at 840 °C"
Formula: Tl2Ba2CaCu2Ox
Informal Name: Tl:2212
Chemical Family: Tl-Ba-Ca-Cu-O
Chemical Class: Oxide
Structure Type:
Manufacturer: In House
Commercial Name: In House
Production Date:
Lot Number:
Production Form: Thin Film
Thermal Expansion for Tl:2212; [Tl-Ba-Ca-Cu-O]
Temperature (K) Thermal Expansion (10-6 K-1)
65 5.5
95 7.6
145 9.7
215 11.7
295 13.3
Measurement Method: X-ray diffraction
The authors cite E.F. Skelton et al., Rev. Sci. Instrum., Vol. 55, 849 (1984), and summarize the procedure as follows. "... the sample was mounted with thermally conducting grease on the cold stage of a Helitran cryogenic refrigerator. This refrigerator system is coupled to a computer controlled x-ray diffractometer... A calibrated Si-diode thermometer is also bonded to the low-temperature block, and coarse temperature control is achieved by regulating the flow rate of He fluid from a remote storage Dewar. Fine control is accomplished with an electrical heater and feed-back circuit... The sample was illuminated with radiation from a Cu x-ray tube and the scattered radiation measured with a NaI(Tl) detector through a graphite monochromator. Data were collected at fixed temperatures in a step-scanning mode over the range from 80° to 100° in 2ϑ."

Cautions: Evaluated Data
Data were digitized from Figure 2 of the paper.