NIST Standard Reference Database 30
Last Update to Data Content: 2002
"Effect of Surface Condition on the Flexural Strength of Sintered Silicon Nitride," J.E.O. Ovri and T.J. Davies, Journal of Materials Science Letters, Vol. 6, pp. 849-850 (1987), published by Chapman and Hall.Language: English
The specimens were sintered. Sintering aids for Material Number 1: 5% MgO. Sintering aids for Material Number 2: 1% MgO and 5% Y2O3. Rectangular beams, 5 mm x 2.5 mm x 30 mm, were tested.
The measurement was made by three-point bend method in air. Instron test machine (Model TT-CM-A0072), crosshead speed = 0.5 mm/min. The reported span of 2.4 mm between supports is questionable. Some specimens were diamond-lapped in the direction parallel to the long axis of the specimen.
| Mass Fraction of Phase ( % ) |
Phase ( no unit ) |
|---|---|
| 95 | Si3N4 |
| 5 | MgO |
| Amount of Element ( formula units ) |
Element ( no unit ) |
|---|---|
| 3 | Si |
| 4 | N |
| Amount of Sintering Aid ( % ) |
Sintering Aid ( no unit ) |
|---|---|
| 5 | MgO |
| Temperature ( °C ) |
Diamond Lapped |
Flexural Strength ( MPa ) |
|---|---|---|
| 23 | no | 561 ± 63 |
| 23 | yes | 442 ± 73 |
| Temperature ( °C ) |
Diamond Lapped |
Weibull Modulus ( no unit ) |
|---|---|---|
| 23 | no | 10.1 ± 1.1 |
| 23 | yes | 6.5 ± 0.8 |
| Temperature ( °C ) |
Diamond Lapped |
Weibull Strength ( MPa ) |
|---|---|---|
| 23 | no | 589 |
| 23 | yes | 474 |
| Mass Fraction of Phase ( % ) |
Phase ( no unit ) |
|---|---|
| 94 | Si3N4 |
| 1 | MgO |
| 5 | Y2O3 |
| Amount of Element ( formula units ) |
Element ( no unit ) |
|---|---|
| 3 | Si |
| 4 | N |
| Amount of Sintering Aid ( % ) |
Sintering Aid ( no unit ) |
|---|---|
| 1 | MgO |
| 5 | Y2O3 |
| Temperature ( °C ) |
Diamond Lapped |
Flexural Strength ( MPa ) |
|---|---|---|
| 23 | no | 421 ± 49 |
| 23 | yes | 423 ± 68 |
| Temperature ( °C ) |
Diamond Lapped |
Weibull Modulus ( no unit ) |
|---|---|---|
| 23 | no | 9.5 ± 0.8 |
| 23 | yes | 6.8 ± 0.7 |
| Temperature ( °C ) |
Diamond Lapped |
Weibull Strength ( MPa ) |
|---|---|---|
| 23 | no | 443 |
| 23 | yes | 452 |