NIST Standard Reference Database 30
Last Update to Data Content: 2002
"Diametral Compression of Silicon Nitride," J.E.O. Ovri and T.J. Davies, Materials Science and Engineering, Vol. 96, pp. 109-116 (1987), published by Elsevier Sequoia.Language: English
"Pressureless sintered silicon nitride (supplied by Turner and Newall Materials Research Limited, Trafford Park, Manchester) was used..." The mass fractions of the sintering aids were 1% MgO and 5 % Y2O3.
The measurements were made by diametral compressive disc test. Testing machine - Instron Model TT-SML-A06-75), crosshead speed = 0.2 mm/min in air. "In its simplest form, a right circular cylindrical specimen is compressed diametrally between two flat platens. ... A biaxial stress state is produced within the test specimen and, on the assumption of ideal line loading, the vertical plane ... is subjected to a uniform horizontal tensile strength of magnitude σt = 2P/(3.14156*d*t) where σt is the maximum tensile stress, P is the applied load at fracture, d is the specimen diameter, and t is the specimen thickness."Three-point bend test
The measurements were made by three-point bend method using an Instron (Model TT-CM-A0072) tester with a crosshead speed = 0.5 mm/min in air. Twenty specimens in the as-sintered condition were used.
| Amount of Element ( formula units ) |
Element ( no unit ) |
|---|---|
| 3 | Si |
| 4 | N |
| Temperature ( °C ) |
Disk Thickness ( mm ) |
Disk Diameter ( mm ) |
Density ( g cm-3 ) |
|---|---|---|---|
| 25 | 4.009 | 20.454 | 2.85 ± 0.13 |
| 25 | 4.299 | 12.587 | 2.82 ± 0.10 |
| 25 | 4.398 | 12.351 | 2.80 ± 0.11 |
| Temperature ( °C ) |
Density ( g cm3 ) |
Flexural Strength ( MPa ) |
|---|---|---|
| 25 | 2.85 ± 0.13 | 421±49 |
| Temperature ( °C ) |
Density ( g/cm3 ) |
Disk Thickness ( mm ) |
Disk Diameter ( mm ) |
Tensile Strength ( MPa ) |
|---|---|---|---|---|
| 25 | 2.85 ± 0.13 | 4.009 | 20.454 | 168 ± 28 |
| 25 | 2.82 ± 0.10 | 4.299 | 12.587 | 111 ± 20 |
| 25 | 2.80 ± 0.11 | 4.398 | 12.351 | 82 ± 7 |