NIST Structural Ceramics Database (SCD) Database

NIST Standard Reference Database 30

Last Update to Data Content: 2002

DOI: http://dx.doi.org/10.18434/T4F30D


SCD Citation Number: Z00015

Bibliographic Information

Reference:
"Tensile Strength Properties of Hot-Pressed Silicon Nitride," T. Ohji, S. Sakai, M. Ito, Y. Yamauchi, W. Kanematsu, and S. Ito, Proceedings of the Thirtieth Japan Congress on Materials Research, pp. 201-206 (1987), published by Society of Materials Science (Japan).
Language: English

General Materials Processing Notes

"Hot pressed silicon nitride with Y2O3 5 wt% and Al2O3 3 wt% was used in this study. The density of this material was 3.199 g/cm3. The plates (80 mm long by 16 mm wide by 3 mm thick) cut from billets of hot-pressed silicon nitride (140 mm long by 140 mm wide by 16 mm thick) were roughly ground by 200 grid diamond wheel into the (dogbone) shape ... and then finished by 400 grid diamond wheel at a feed speed of 2 mm/min with a cutting depth of 20 µm. In addition, the gauge length areas of specimens were hand polished with 2000 grid diamond paste and the surface layer of 50 µm thickness was removed... The bending specimens (36 mm long by 4 mm wide by 3 mm thick) were cut from the billets so that the tensile face was perpendicular to the hot-pressing direction. All faces were ground lengthwise using a 400 grid diamond wheel and edges were chamfered using an 800 grind diamond whetstone."

Measurement Methods

Three-point bend test
The measurements were made by three-point bend method. The span length was 30 mm and the crosshead speed was 0.2 mm/min. Test were conducted in air.
Tensile test
The measurements were made by tensile test method. Test jig pins were made of SiC; the universal joint and specimen holder and pull rod were made of molybdenum; and the crosshead speed was 0.1 mm/min in air.
Analysis
Weibull analysis was used for both flexural and tensile test results which were obtained by the three-point bending and tensile tests repectively.

Index of Materials and Properties

SCD Citation Number: Z00015
Material Number 1: Si3N4·xAl2O3·yY2O3

Material Specification and Properties for Si3N4·xAl2O3·yY2O3

Material number 1 of 1
in SCD Citation Number: Z00015
Chemical Class: Nitride
Chemical Family: Si-N:Al2O3,Y2O3
Formula: Si3N4·xAl2O3·yY2O3
Informal Name: silicon nitride
Structure Type: Polycrystalline
Manufacturer: In-House
Process: Hot Pressing

Si3N4·xAl2O3·yY2O3

Material number 1 of 1
in SCD Citation Number: Z00015
Elemental Composition
Amount of
Element
( formula units )
Element
 
( no unit )
3 Si
4 N
Measurement Method: Reported Formula
Evaluation Status: Certified standard reference values

Si3N4·xAl2O3·yY2O3

Material number 1 of 1
in SCD Citation Number: Z00015
Flexural Strength
Temperature
 
( °C )
Environment
 
 
Flexural
Strength
( MPa )
22 air 1030
800 vacuum 770
1000 vacuum 800
1200 vacuum 510
1400 vacuum 160

Measurement Method: Three-point bend test
Evaluation Status: Evaluated by acceptance criteria
Cautions:
Digitized data were obtained from Figure 6 of the paper.

Si3N4·xAl2O3·yY2O3

Material number 1 of 1
in SCD Citation Number: Z00015
Tensile Strength
Temperature
 
( °C )
Environment
 
 
Tensile
Strength
( MPa )
22 air 760
800 vacuum 700
1000 vacuum 720
1200 vacuum 370
1400 vacuum 50

Measurement Method: Tensile test
Evaluation Status: Evaluated by acceptance criteria
Cautions:
Digitized data were obtained from Figure 6 of the paper.

Si3N4·xAl2O3·yY2O3

Material number 1 of 1
in SCD Citation Number: Z00015
Weibull Modulus
Temperature
 
( °C )
Environment
 
 
Strength
Mode
 
Weibull
Modulus
( no unit )
22 air Flexure 14.2
1200 vacuum Flexure 25.7
22 air Tension 8.6
1200 vacuum Tension 20.0

Measurement Method: Analysis
Evaluation Status: Evaluated by acceptance criteria