NIST Structural Ceramics Database (SCD) Database

NIST Standard Reference Database 30

Last Update to Data Content: 2002

DOI: http://dx.doi.org/10.18434/T4F30D


SCD Citation Number: Z00016

Bibliographic Information

Reference:
"Effect of Hot Isostatic Pressing on the Properties of Sintered Alpha Silicon Carbide," G.K. Watson, T.J. Moore, and M.L. Millard, American Ceramic Society Bulletin, Vol. 64 [9], pp. 1253-1256 (1985), published by American Ceramic Society.
Language: English

General Materials Processing Notes

"Two lots of alpha-SiC (Carborundum Co., Niagara Falls, NY) rectangular blocks were evaluated. Lot 1 blocks had dimensions of 5.0 cm by 5.0 cm by 0.5 cm. Lot 2 blocks were obtained in two sizes. The thin blocks had dimensions of 5.0 cm by 5.0 cm by 0.5 cm, whereas the thick blocks had dimensions of 5.0 cm by 5.0 cm by 1.3 cm. ... Because of the high density (greater than 95% TD) of the sintered alpha-SiC for both lots of the as-received materials, no external cladding was needed for HIPing. The blocks and/or bars were placed in high purity SiC sand in a carbon crucible and inserted into the HIP. The specimens were HIPed in Ar under 138 MPa pressure. All specimens were given a 2 h soak at a HIPing temperature ranging from 1850 °C to 2200 °C for lot 1 materials or from 1950 °C to 2200 °C for lot 2 materials. All HIPed blocks were then diamond saw cut and ground into MOR test bars (2.50 cm by 0.63 cm by 0.31 cm)."

Measurement Methods

Archimedes' method
"The density was determined in all the bars by the water immersion method."
Four-point bend test
"...4-point, 1/4-point (inner span 0.95 cm, outer span 1.9 cm) room temperature and 1200 °C bend strengths were evaluated." No additional measurement details were noted.
SEM image analysis
"Polished sections ... were examined using an image analyzer ..." No additional measurement details were noted.

Index of Materials and Properties

SCD Citation Number: Z00016
Material Number 1: SiC

Material Specification and Properties for SiC

Material number 1 of 1
in SCD Citation Number: Z00016
Chemical Class: Carbide
Chemical Family: Si-C
Formula: SiC
Informal Name: silicon carbide
Structure Type: Polycrystalline
Manufacturer: Carborundum Company
Process: Hot Isostatic Pressing

SiC

Material number 1 of 1
in SCD Citation Number: Z00016
Elemental Composition
Amount of
Element
( formula units )
Element
 
( no unit )
1 Si
1 C

Measurement Method: Reported Formula
Evaluation Status: Unevaluated

SiC

Material number 1 of 1
in SCD Citation Number: Z00016
Density (mass)
HIP
Temperature
( °C )
Test
Temperature
( °C )
Lot
Number
 
Density
 
( g cm-3 )
--- 22 1 3.10 ± 0.01
1850 22 1 3.11
1950 22 1 3.13
2050 22 1 3.15
2200 22 1 3.16
--- 22 2 3.04
1950 22 2 3.07
2050 22 2 3.15
2200 22 2 3.15

<Measurement Method: Archimedes' method
Evaluation Status: Evaluated by acceptance criteria
Cautions:
Digitized data were obtained from Figure 1 of the paper.

SiC

Material number 1 of 1
in SCD Citation Number: Z00016
Flexural Strength
Number of
Specimens
 
HIP
Temperature
( °C )
Test
Temperature
( °C )
Lot
Number
 
Flexural
Strength
( MPa )
32 --- 22 1 500 ± 75
6 1850 22 1 530 ± 70
5 1950 22 1 470 ± 80
9 2050 22 1 570 ± 30
39 2200 22 1 530 ± 50
20 --- 22 2 425 ± 70
19 1950 22 2 430 ± 60
14 2050 22 2 500 ± 90
31 2200 22 2 520 ± 45
57 --- 1200 1 430 ± 110
6 1850 1200 1 440 ± 70
6 1950 1200 1 415 ± 70
9 2050 1200 1 535 ± 60
20 2200 1200 1 585 ± 80
22 --- 1200 2 365 ± 75
10 1950 1200 2 365 ± 50
5 2050 1200 2 540 ± 90
15 2200 1200 2 580 ± 30

Measurement Method: Four-point bend test
Evaluation Status: Unevaluated
Cautions:
Digitized data were obtained from Figure 2 of the paper.

SiC

Material number 1 of 1
in SCD Citation Number: Z00016
Grain Size
Average
Pore Size
( µm )
HIP
Temperature
( °C )
Lot
Number
 
Grain Size
 
( µm )
1.9 --- 1 4
2.1 1950 1 4
1.4 2050 1 6
1.8 2200 1 7
2.0 --- 2 4
2.1 1950 2 4
1.5 2050 2 5
1.6 2200 2 5
Measurement Method: SEM image analysis
Evaluation Status: Unevaluated

SiC

Material number 1 of 1
in SCD Citation Number: Z00016
Weibull Modulus
HIP
Temperature
( °C )
Test
Temperature
( °C )
Lot
Number
 
Weibull
Modulus
( no unit )
--- 22 1 6.4
2200 22 1 11.5
--- 22 2 6.2
2200 22 2 12.3
--- 1200 1 3.8
2200 1200 1 7.5
--- 1200 2 5.1
2200 1200 2 12.0

Measurement Method: Four-point bend test
Evaluation Status: Unevaluated