NIST Standard Reference Database 30
Last Update to Data Content: 2002
"Effect of Hot Isostatic Pressing on the Properties of Sintered Alpha Silicon Carbide," G.K. Watson, T.J. Moore, and M.L. Millard, American Ceramic Society Bulletin, Vol. 64 [9], pp. 1253-1256 (1985), published by American Ceramic Society.Language: English
"Two lots of alpha-SiC (Carborundum Co., Niagara Falls, NY) rectangular blocks were evaluated. Lot 1 blocks had dimensions of 5.0 cm by 5.0 cm by 0.5 cm. Lot 2 blocks were obtained in two sizes. The thin blocks had dimensions of 5.0 cm by 5.0 cm by 0.5 cm, whereas the thick blocks had dimensions of 5.0 cm by 5.0 cm by 1.3 cm. ... Because of the high density (greater than 95% TD) of the sintered alpha-SiC for both lots of the as-received materials, no external cladding was needed for HIPing. The blocks and/or bars were placed in high purity SiC sand in a carbon crucible and inserted into the HIP. The specimens were HIPed in Ar under 138 MPa pressure. All specimens were given a 2 h soak at a HIPing temperature ranging from 1850 °C to 2200 °C for lot 1 materials or from 1950 °C to 2200 °C for lot 2 materials. All HIPed blocks were then diamond saw cut and ground into MOR test bars (2.50 cm by 0.63 cm by 0.31 cm)."
"The density was determined in all the bars by the water immersion method."Four-point bend test
"...4-point, 1/4-point (inner span 0.95 cm, outer span 1.9 cm) room temperature and 1200 °C bend strengths were evaluated." No additional measurement details were noted.SEM image analysis
"Polished sections ... were examined using an image analyzer ..." No additional measurement details were noted.
| Amount of Element ( formula units ) |
Element ( no unit ) |
|---|---|
| 1 | Si |
| 1 | C |
| HIP Temperature ( °C ) |
Test Temperature ( °C ) |
Lot Number |
Density ( g cm-3 ) |
|---|---|---|---|
| --- | 22 | 1 | 3.10 ± 0.01 |
| 1850 | 22 | 1 | 3.11 |
| 1950 | 22 | 1 | 3.13 |
| 2050 | 22 | 1 | 3.15 |
| 2200 | 22 | 1 | 3.16 |
| --- | 22 | 2 | 3.04 |
| 1950 | 22 | 2 | 3.07 |
| 2050 | 22 | 2 | 3.15 |
| 2200 | 22 | 2 | 3.15 |
Digitized data were obtained from Figure 1 of the paper.
| Number of Specimens |
HIP Temperature ( °C ) |
Test Temperature ( °C ) |
Lot Number |
Flexural Strength ( MPa ) |
|---|---|---|---|---|
| 32 | --- | 22 | 1 | 500 ± 75 |
| 6 | 1850 | 22 | 1 | 530 ± 70 |
| 5 | 1950 | 22 | 1 | 470 ± 80 |
| 9 | 2050 | 22 | 1 | 570 ± 30 |
| 39 | 2200 | 22 | 1 | 530 ± 50 |
| 20 | --- | 22 | 2 | 425 ± 70 |
| 19 | 1950 | 22 | 2 | 430 ± 60 |
| 14 | 2050 | 22 | 2 | 500 ± 90 |
| 31 | 2200 | 22 | 2 | 520 ± 45 |
| 57 | --- | 1200 | 1 | 430 ± 110 |
| 6 | 1850 | 1200 | 1 | 440 ± 70 |
| 6 | 1950 | 1200 | 1 | 415 ± 70 |
| 9 | 2050 | 1200 | 1 | 535 ± 60 |
| 20 | 2200 | 1200 | 1 | 585 ± 80 |
| 22 | --- | 1200 | 2 | 365 ± 75 |
| 10 | 1950 | 1200 | 2 | 365 ± 50 |
| 5 | 2050 | 1200 | 2 | 540 ± 90 |
| 15 | 2200 | 1200 | 2 | 580 ± 30 |
Digitized data were obtained from Figure 2 of the paper.
| Average Pore Size ( µm ) |
HIP Temperature ( °C ) |
Lot Number |
Grain Size ( µm ) |
|---|---|---|---|
| 1.9 | --- | 1 | 4 |
| 2.1 | 1950 | 1 | 4 |
| 1.4 | 2050 | 1 | 6 |
| 1.8 | 2200 | 1 | 7 |
| 2.0 | --- | 2 | 4 |
| 2.1 | 1950 | 2 | 4 |
| 1.5 | 2050 | 2 | 5 |
| 1.6 | 2200 | 2 | 5 |
| HIP Temperature ( °C ) |
Test Temperature ( °C ) |
Lot Number |
Weibull Modulus ( no unit ) |
|---|---|---|---|
| --- | 22 | 1 | 6.4 |
| 2200 | 22 | 1 | 11.5 |
| --- | 22 | 2 | 6.2 |
| 2200 | 22 | 2 | 12.3 |
| --- | 1200 | 1 | 3.8 |
| 2200 | 1200 | 1 | 7.5 |
| --- | 1200 | 2 | 5.1 |
| 2200 | 1200 | 2 | 12.0 |