NIST Standard Reference Database 30
Last Update to Data Content: 2002
"Properties of Hot-Pressed Barium-Doped SiC," T. Sakai and N. Hirosaki, Journal of Materials Science Letters, Vol. 5 [1], pp. 43-44 (1986), published by Chapman and Hall.Language: English
"...silicon carbide is densified by hot-pressing, adding barium oxide and carbon simultaneously. The powder with 3 % to 5 % (mass fraction) of BaO and 0.6 % to 2 % of carbon in the ratio 4:5 of the two additives, respectively, was densified to obtain compacts denser than 3.0 g/cm3. ...the SiC specimen (10 mm diameter and about 2 mm thick), (was) hot-pressed in a vacuum under a pressure of 20 MPa at 2050 °C for 30 min."
The authors cite W.J. Parker et al., Journal of Applied Physics, Vol. 32, 1679 (1961), and summarize the procedure as follows. "Thermal diffusivity... was measured using the laser flash method at 298 K. Thermal conductivity, k, was then calculated by k = αCpd where α is the measured thermal diffusivity, d is the density, and Cp is the specific heat of the material. The value used for Cp was 0.66 J g-1 K-1. Corrections were made for the porosity of the compact..."Three-point bend test
"Test pieces for three-point flexural strength of the compacts, 2.8 mm x 3.5 mm x 25 mm, were cut from the disk of 33 mm diameter and about 4 mm thick and ground with a 60 µm diamond grinding wheel. The test load was applied over a 20 mm span at a crosshead spead of 0.5 mm min-1 at room temperature using a universal tester in the direction that hot pressing had been performed."
| Amount of Element ( formula units ) |
Element ( no unit ) |
|---|---|
| 1 | Si |
| 1 | C |
| Mass Fraction of BaO ( % ) |
Mass Fraction of free C ( % ) |
Density ( g cm-3 ) |
|---|---|---|
| 0.0 | 1.0 | 2.49 |
| 1.0 | 1.0 | 2.49 |
| 3.0 | 1.0 | 3.00 |
| 5.0 | 1.0 | 3.06 |
| 10.0 | 1.0 | 2.72 |
| 5.0 | 0.0 | 1.84 |
| 5.0 | 0.3 | 2.19 |
| 5.0 | 1.0 | 3.04 |
| 5.0 | 2.0 | 2.90 |
No measurement details were noted. Digitized data were obtained from Figure 1 of the paper.
| Temperature ( °C ) |
Mass Fraction of BaO ( % ) |
Mass Fraction of free C ( % ) |
Flexural Strength ( MPa ) |
|---|---|---|---|
| 22 | 5 | 1 | 216 |
| Mass Fraction of BaO ( % ) |
Mass Fraction of free C ( % ) |
Thermal Conductivity ( W m-1 K-1 ) |
|---|---|---|
| 0.0 | 1.0 | 121 |
| 1.0 | 1.0 | 85 |
| 3.0 | 1.0 | 61 |
| 5.0 | 1.0 | 20 |
| 10.0 | 1.0 | 20 |
| 5.0 | 0.2 | 120 |
| 5.0 | 1.0 | 20 |
| 5.0 | 2.0 | 13 |
Digitized data were obtained from Figure 1 of the paper.