NIST Structural Ceramics Database (SCD) Database

NIST Standard Reference Database 30

Last Update to Data Content: 2002

DOI: http://dx.doi.org/10.18434/T4F30D


SCD Citation Number: Z00025

Bibliographic Information

Reference:
"The Fabrication and Properties of Self-Bonded Silicon Carbide Bodies," C.W. Forrest, P. Kennedy, and J.V. Shennan, Special Ceramics, Vol. 5, pp. 99-123 (1972), published by The British Ceramic Research Association.
Language: English

General Materials Processing Notes

"The α-SiC and graphite powders are firstly dry blended in a Y-cone mixer. To this mix is added a weighed amount of a binder, containing a thermoplastic polymer and plasticizer in varing amounts dispersed in a solvent, and a small weighed amount of thermosetting resin, and the whole mix is slurried with an excess of methylethylketone to ensure a uniform distribution of the binder. The slurry is vacuum dried and at a suitable stage in the drying operation the cake is broken up to a friable powder. Drying is continued until the binder plus solvent reaches a preset weight, then the mix is removed and compacted. ... The mix is pressed to give cylindrical equi-axed compacts and then pre-extruded as (2.54 mm = 0.1 in.) diameter rod through a multi-hole extrusion plate. ... The extruded material is cut to length and loaded in graphite V-blocks for removal of binder by heating to 370°C in air. ... The reaction sintering process is performed under vacuum in a graphite crucible heated by induction. ... At 1410°C the silicon melts, is transported to the base of the compacts by surface wetting and rises through them, reacting with the graphite, the temperature being allowed to reach 1600-1700°C. When the reaction is complete, the crucible is allowed to cool to room temperature and the silicided material is removed."

Measurement Methods

Three-point bend test
"The modulus of rupture of self-bonded silicon carbide has been measured in air under three-point loading. An average value of 424 MPa with a standard deviation of... 30 MPa was obtained...at room temperature." No additional measurement details were noted.

Index of Materials and Properties

Material Number 1: SiC

Material Specification and Properties for SiC

Material number 1 of 1
in SCD Citation Number: Z00025
Chemical Class: Carbide
Chemical Family: Si-C
Formula: SiC
Informal Name: silicon carbide
Structure Type: Polycrystalline
Manufacturer: Reactor Fuel Element Laboratories
Production Form: Rod
Process: Reaction Bonding

SiC

Material number 1 of 1
in SCD Citation Number: Z00025
Elemental Composition
Amount of
Element
( formula units )
Element
 
( no unit )
1 Si
1 C

Measurement Method: Reported Formula
Evaluation Status: Unevaluated

SiC

Material number 1 of 1
in SCD Citation Number: Z00025
Density (mass)
Density
 
( g cm-3 )
3.12 ± 0.02

Measurement Method: Unknown
Evaluation Status: Unevaluated
Cautions:
No measurement details were noted.

SiC

Material number 1 of 1
in SCD Citation Number: Z00025
Elastic Modulus
Elastic
Modulus
( GPa )
420

Measurement Method: Unknown
Evaluation Status: Unevaluated
Cautions:
No measurement details were noted.

SiC

Material number 1 of 1
in SCD Citation Number: Z00025
Flexural Strength
Temperature
 
( °C )
Flexural
Strength
( MPa )
25 424
200 504
400 535
600 563
800 557
1000 563
1150 554
1250 554
1350 582
1400 227
1450 257

Measurement Method: Three-point bend test
Evaluation Status: Unevaluated
Cautions:
Digitized data were obtained from Figure 12 of the paper.

SiC

Material number 1 of 1
in SCD Citation Number: Z00025
Poisson's Ratio
Poisson's
Ratio
( no unit )
0.166

Measurement Method: Unknown
Evaluation Status: Unevaluated
Cautions:
No measurement details were noted.

SiC

Material number 1 of 1
in SCD Citation Number: Z00025
Thermal Conductivity
Temperature
 
( °C )
Thermal
Conductivity
( W m-1 K-1 )
300 91
400 75
590 57
800 36
980 18
1190 13

Measurement Method: Unknown
Evaluation Status: Unevaluated
Cautions:
No measurement details were noted. Digitized data were obtained from Figure 11 of the paper.

SiC

Material number 1 of 1
in SCD Citation Number: Z00025
Thermal Expansion
Temperature
Range
( °C )
Thermal
Expansion
( 10-6 K-1 )
20 - 1000 4.4

Measurement Method: Unknown
Evaluation Status: Unevaluated
Cautions:
No measurement details were noted.