NIST Standard Reference Database 30
Last Update to Data Content: 2002
"Hot Isostatic Press Sintering and Properties of Silicon Nitride without Additives," I. Tanaka, G. Pezzotti, T. Okamoto, and Y. Miyamoto, Journal of the American Ceramic Society, Vol. 72 [9], pp. 1656-1660 (1989), published by American Ceramic Society.Language: English
Ube E-10 powder was compacted by uniaxial pressing at 20 MPa and cold isostatic pressing at 200 MPa. The compact was coated with BN powder and prefired at 1200 °C in vacuum. Then, encapsulated in borosilicate glass tubes, hot isostatic pressing was done at 2000 °C, 170 MPa in argon gas for one hour.hr/>
Four-point bend tests with inner and outer spans of 10 mm and 30 mm and a crosshead speed of 0.5 mm/min were performed in air. Bars of dimensions 3 mm x 4 mm x 34 mm were used. The specimen surface was ground with a 400-grit diamond wheel.Vickers indentation
The authors cite K. Niihara et al., J. Am. Cer. Soc., Vol. 65, C-116 (1982) and summarize the procedure as follows. The Vickers microindentation method was used with loads of 9.8 N to 49 N applied with a loading rate of 0.2 mm/s. The maximum load was applied for 15 s.Mechanical resonance
The authors cite K. Matsushita et al., J. Mater. Sci. Letter, Vol.3, 345-348 (1984) and summarize the procedure as follows. Specimens were 2 mm x 8 mm x 34 mm. The resonant frequency was 17 kHz.
| Amount of Phase ( % ) |
Phase ( no unit ) |
|---|---|
| 100 | βSi3N4 |
| Amount of Element ( formula units ) |
Element ( no unit ) |
|---|---|
| 3 | Si |
| 4 | N |
| Temperature ( °C ) |
Elastic Modulus ( GPa ) |
|---|---|
| 22 | 312.2 |
| 100 | 312.4 |
| 200 | 312.0 |
| 300 | 311.5 |
| 400 | 310.6 |
| 500 | 309.6 |
| 600 | 308.5 |
| 700 | 307.3 |
| 800 | 305.9 |
| 900 | 304.5 |
Data were digitized from Fig. 7 of the paper with a resolution of ±0.1 GPa.
| Temperature ( °C ) |
Flexural Strength ( MPa ) |
|---|---|
| 22 | 544 |
| 1000 | 523 |
| 1400 | 523 |
Data were digitized from Fig. 5 of the paper, with a resolution of ±3 MPa.
| Temperature ( °C ) |
Fracture Toughness ( MPa m1/2 ) |
|---|---|
| 22 | 3.12 |
| 200 | 3.18 |
| 500 | 2.85 |
| 800 | 2.83 |
| 1000 | 2.59 |
| 1100 | 2.61 |
| 1200 | 2.58 |
Data were digitized from Fig. 6 of the paper, with a resolution of ±0.05 MPa·m1/2.
| Temperature ( °C ) |
Hardness ( GPa ) |
|---|---|
| 22 | 14.6 |
| 200 | 14.4 |
| 500 | 13.0 |
| 800 | 11.0 |
| 900 | 11.5 |
| 1000 | 11.5 |
| 1100 | 10.8 |
| 1200 | 10.2 |
Data were digitized from figure 4 of the paper, with a resolution of ±0.2 GPa.