NIST Structural Ceramics Database (SCD) Database

NIST Standard Reference Database 30

Last Update to Data Content: 2002

DOI: http://dx.doi.org/10.18434/T4F30D


SCD Citation Number: Z00054

Bibliographic Information

Reference:
"Test Metodology for Tubular Components," J.C. Conway, J.J. Mecholsky, and S.M. Wiederhorn, Projects Within the Center for Advanced Materials, pp. 201-276 (1990), edited by J.R. Hellmann and B.K. Kennedy, published by Center for Advanced Materials, Pennsylvania State University.
Language: English
Notes: June 1, 1988 to May 31, 1989 (CAM-8904)

General Materials Processing Notes

Commercially available silicon carbide materials were used in this study.

Measurement Methods

Compression test
The authors cite D.L. Shelleman, "Test Methodology for Tubular Ceramics (Fast Fracture Strength Study)", Ph.D. Thesis, The Pennsylvania State University, University Park, PA, May 1991, and summarize the procedure as follows. Rings were cut from tubes 0.381±0.013 mm oversized using a 220-grit cut-off wheel. The sides of the rings were subsequently ground using a 220-grit wheel to within 0.076-0.127 mm of final dimensions. Material removal rate was less than or equal to 0.013 mm per pass. The sides of the rings were then lapped to final dimension using 15 µm sized media. Both inner and outer surface of the rings remained in the as-received condition. Final O-ring dimensions were: 43.8±0.4 mm O.D. x 34.2±0.3 mm I.D. x 9.5 mm for SCRB210; and 44.4±0.9 mm O.D. x 34.9±0.7 mm I.D. x 9.5 mm for Hexoloy SA. Final C-ring dimensions were: 44.4±0.9 mm O.D. x 34.9±0.7 mm I.D. x 9.5 mm wide for Hexoloy SA. A 1.6 mm stripe of alumina felt was placed between the ring specimen and the alumina loading rams. A 2.27 kg pre-load was applied to the specimen to maintain alignment. For room temperature testing, the rings were then loaded to failure at a crosshead rate of 0.508 mm/min. For elevated temperature testing, a computer was interfaced with the Instron testing machine and programmed to maintain the preload during transient heating to the test temperature. This compensated for thermal expansion of the specimen and loading train. Once the test temperature was reached the load was increased to 4.54 kg and held for 15 min. to allow the specimen to thermally equilibrate. Then specimens were loaded to failure using a crosshead rate of 0.508 mm/min.

Index of Materials and Properties

SCD Citation Number: Z00054

Material Specification and Properties for SiC

Material number 1 of 2
in SCD Citation Number: Z00054
Chemical Class: Carbide
Chemical Family: Si-C
Formula: SiC
Informal Name: silicon carbide
Structure Type: Polycrystalline
Manufacturer: Coors Porcelain Company
Commercial Name: SCRB210
Production Form: Tube
Process: Reaction Bonding

SiC

Material number 1 of 2
in SCD Citation Number: Z00054
Elemental Composition
Amount of
Element
( formula units )
Element
 
( no unit )
1 Si
1 C
Measurement Method: Reported Formula
Evaluation Status: Unevaluated

SiC

Material number 1 of 2
in SCD Citation Number: Z00054
Compressive Strength
Temperature
 
( °C )
Test
Type
 
Compressive
Strength
( GPa )
25 O-ring 265 ± 24
800 O-ring 277 ± 28
1000 O-ring 305 ± 20
1200 O-ring 321 ± 20
1300 O-ring 325 ± 24
Measurement Method: Compression test
Evaluation Status: Evaluated by acceptance criteria

SiC

Material number 1 of 2
in SCD Citation Number: Z00054
Weibull Modulus
Temperature
 
( °C )
Test
Type
 
Weibull
Modulus
( no unit )
25 O-ring 5.5
800 O-ring 4.8
1000 O-ring 7.6
1200 O-ring 7.3
1300 O-ring 7.2
Measurement Method: Compression test
Evaluation Status: Evaluated by acceptance criteria

Material Specification and Properties for SiC

Material number 2 of 2
in SCD Citation Number: Z00054
Chemical Class: Carbide
Chemical Family: Si-C
Formula: SiC
Informal Name: silicon carbide
Structure Type: Polycrystalline
Manufacturer: Sohio Engineered Materials Co.
Commercial Name: Hexoloy SA
Production Form: Tube
Process: Sintering

SiC

Material number 2 of 2
in SCD Citation Number: Z00054
Elemental Composition
Amount of
Element
( formula units )
Element
 
( no unit )
1 Si
1 C
Measurement Method: Reported Formula
Evaluation Status: Unevaluated

SiC

Material number 2 of 2
in SCD Citation Number: Z00054
Compressive Strength
Temperature
 
( °C )
Test
Type
 
Compressive
Strength
( GPa )
25 O-ring 294 ± 16
1200 O-ring 302
1300 O-ring 300
1400 O-ring 300
25 C-ring 241 ± 10
1200 C-ring 261 ± 14
1300 C-ring 268 ± 20
1400 C-ring 290 ± 14
1400 C-ring 290±14
Measurement Method: Compression test
Evaluation Status: Evaluated by acceptance criteria

SiC

Material number 2 of 2
in SCD Citation Number: Z00054
Weibull Modulus
Temperature
 
( °C )
Test
Type
 
Weibull
Modulus
( no unit )
25 O-ring 12.5
1200 O-ring 13.3
1300 O-ring 10.3
1400 O-ring 12.6
25 C-ring 15.2
1200 C-ring 10.1
1300 C-ring 6.9
1400 C-ring 12.9
Measurement Method: Compression test
Evaluation Status: Evaluated by acceptance criteria