NIST Structural Ceramics Database (SCD) Database

NIST Standard Reference Database 30

Last Update to Data Content: 2002

DOI: http://dx.doi.org/10.18434/T4F30D


SCD Citation Number: Z00361

Bibliographic Information

Reference:
"Ceramic Technology Project Data Base: September 1992 Summary Report," B.L.P. Keyes, ORNL Report Number: ORNL/M-2775, pp. 1-171 (1992), published by Oak Ridge National Laboratory.
Language: English
Notes: DOE Materials Database: Y-TZP

General Materials Processing Notes

SCD Citation Number: Z00361
Material Designation: Y-TZP Primary Matrix: ZrO2 Specimen A: Additives: 4.66 wt% Y2O3 Densification Process: SINTERED/1500C/207MPa Specimen B,C: Additives: 5.27 wt% Y2O3 Densification Process: SINTERED/1500C/207MPa Specimen D: Additives: 5.52 wt% Y2O3 Densification Process: SINTERED/1500C/207MPa Specimen E: Additives: 4.7 wt% Y2O3 Densification Process: SINTERED/1500C/207MPa Specimen F: Additives: 4.53 wt% Y2O3 + 1.91 wt% CeO2 Densification Process: SINTERED/1500C/207MPa Specimen G: Additives: 4.49 wt% Y2O3 + 3.99 wt% CeO2 Densification Process: SINTERED/1500C/207MPa Specimen H: Additives: 4.7 wt% Y2O3 Densification Process: SINTERED/1500C/207MPa General Notes: "Yttria and Ce-doped ZrO2 were prepared by arc-melting and rapid solidification. The crude material was then vibratory milled (Sweco) to produce average sizes of 0.4 µm, 0.5 µm, and 0.7 µm. Powder was then dry-pressed and CIPed at 207 MPa and fired at 1500 °C. A few billets were also gas-pressure sintered at 1500 °C."

Measurement Methods

Four-point bend test
"Specimens 3.175 mm x 3.25 mm x 35 mm were machined from fired billets, then broken in a 4-point bend fixture using an inner span of 12.7 mm, outer span of 25.4 mm. Tests at room temperature were run at a crosshead speed of 0.0085 mm/s, while tests at elevated temperatures used a faster crosshead speed (see test results for specifics)."

Index of Materials and Properties

Material Number 1: ZrO2·xY2O3·yCeO2

Material Specification and Properties for ZrO2·xY2O3·yCeO2

Material number 1 of 1
in SCD Citation Number: Z00361
Chemical Class: Oxide
Chemical Family: Zr-O:CeO2,Y2O3
Formula: ZrO2·xY2O3·yCeO2
Informal Name: zirconia (TZP)
Structure Type: Polycrystalline
Manufacturer: Norton Company
Commercial Name: Y-TZP
Process:

ZrO2·xY2O3·yCeO2

Material number 1 of 1
in SCD Citation Number: Z00361
Elemental Composition
Amount of
Element
( formula units )
Element
 
( no unit )
1 Zr
2 O

Measurement Method: Reported Formula
Evaluation Status: Unevaluated

ZrO2·xY2O3·yCeO2

Material number 1 of 1
in SCD Citation Number: Z00361
Flexural Strength
Temperature
 
( °C )
Heat
Treatment
 
Specimen
Number
 
Flexural
Strength
( MPa )
22 -- A 1164
22 -- C 1220
22 -- D 909
25 HIP D 1600 ± 8
300 HIP D 1347 ± 10
500 HIP D 800 ± 12
700 HIP D 576 ± 24
25 SINTERED D 944 ± 22
300 SINTERED D 958 ± 14
500 SINTERED D 653 ± 17
700 SINTERED D 465 ± 22
22 -- E 1137
25 HIP H 1285 ± 36
300 HIP H 1174 ± 41
500 HIP H 896 ± 32
700 HIP H 576 ± 59
25 SINTERED H 1146 ± 29
300 SINTERED H 1146 ± 6
500 SINTERED H 750 ± 19
700 SINTERED H 563 ± 15
25 HIP F 1146 ± 41
300 HIP F 1250 ± 22
500 HIP F 917 ± 17
700 HIP F 562 ± 26
25 SINTERED F 986 ± 17
300 SINTERED F 868 ± 28
500 SINTERED F 590 ± 26
700 SINTERED F 465 ± 18
25 HIP G 1035 ± 20
300 HIP G 938 ± 17
500 HIP G 590 ± 18
700 HIP G 347 ± 12
25 SINTERED G 806 ± 16
300 SINTERED G 700 ± 12
500 SINTERED G 510 ± 15
700 SINTERED G 366 ± 13

Measurement Method: Four-point bend test
Evaluation Status: Evaluated by acceptance criteria

ZrO2·xY2O3·yCeO2

Material number 1 of 1
in SCD Citation Number: Z00361
Fracture Toughness
Temperature
 
( °C )
Environment
 
 
Specimen
Number
 
Fracture
Toughness
( MPa m1/2 )
25 ControlledFlaw A 7.30
25 Double Torsion A 7.60
25 Microindent A 8.80
25 ControlledFlaw B 6.20
25 ControlledFlaw B 6.20
25 ControlledFlaw B 6.40
25 Microindent B 7.90
25 Microindent B 8.30
25 Microindent B 8.40
25 ControlledFlaw D 6.20
25 Microindent D 7.80
25 Microindent D 8.30
25 ControlledFlaw G 5.30

Measurement Method: Unknown
Evaluation Status: Unevaluated
Cautions:
No measurement details were noted.