NIST Structural Ceramics Database (SCD) Database

NIST Standard Reference Database 30

Last Update to Data Content: 2002

DOI: http://dx.doi.org/10.18434/T4F30D


SCD Citation Number: Z00430

Bibliographic Information

Reference:
"Fracture Toughness of Ceramics using the SEVNB Method: Preliminary Results," J. Kubler, Ceramic Engineering and Science Proceedings, Vol. 18 [4], pp. 155-162 (1997), published by American Ceramic Society.
Language: English

General Materials Processing Notes

"Eight advaned ceramics... were tested:... hot pressed silicon nitride (NC-132),... hot-isostatic pressed silicon nitride (HSN),... sintered and post-hipped, 3 mole% yttria-stabilised tetragonal zirconia (Y-TZP) with an average grain size of 0.45 µm,... silicon carbide whisker (20 vol%) reinforced silicon nitride (CMC),... alumina (Al2O3) with an average grain size of 16 µm,... sintered silicon carbide (SSiC) with an average grain size of 7 µm,... hot pressed silicon nitride (HPSN), and... magnesium partially stabilised zirconia (Mg-PSZ) with an average grain size of 60 µm..."

Measurement Methods

Unlisted
No measurement information was noted.
> Single-edge V-notched beam
"Large standard 3 mm x 4 mm x 45 mm specimens with four point spans of S1 = 40 mm and S2 = 20 mm were used for (most) flexure testing. ... small specimens 2 mm x 2.5 mm x (22 to 25) mm were tested with spans of 20 mm and 10 mm, respectively. All specimens were tested on their 3 mm and 2 mm wide faces for the large and small specimens, respectively. At least 5 specimens were tested from each ceramic. Before testing, a straight notch was introduced into the centre of the specimens tensile surface. The total depth of the notches was between 0.8 mm and 1.2 mm for the large specimen and between 0.5 mm and 0.75 mm for the small specimen. The notches were produced either by hand or machining. ... By Hand:... A straight notch was cut with a 200 µm wide diamond wheel to a depth of about 50% of the final depth. ... A second notch was polished into the first one using the slot as a guide. The polishing was done by hand with a razor blade sprinkled with a 4 µm diamond paste. By Machine: A straight notch was polished with the machine and razor blade sprinkled with a 4 µm diamond paste. ... After cleaning the specimen(s), 10% of the final notch depth was polished using a new razor blade sprinkled with a 1 µm diamond paste."

Index of Materials and Properties (Click on a selected Material Number to expand material properties menu)

Material Specification and Properties for Si3N4

Material number 1 of 8
in SCD Citation Number: Z00430
Chemical Class: Nitride
Chemical Family: Si-N
Formula: Si3N4
Informal Name: silicon nitride
Structure Type: Polycrystalline
Manufacturer: Norton Company
Commercial Name: NC-132
Process: Hot Pressing

Si3N4

Material number 1 of 8
in SCD Citation Number: Z00430
Fracture Toughness
Specimen
Size
( mm x mm )
Notch
Polishing
 
Fracture
Toughness
( MPa m1/2 )
3 x 4 machine 4.36 ± 0.08
2 x 2.5 machine 4.36 ± 0.08
Measurement Method: Unlisted
Evaluation Status: Evaluated by acceptance criteria

Material Specification and Properties for Si3N4

Material number 2 of 8
in SCD Citation Number: Z00430
Chemical Class: Nitride
Chemical Family: Si-N
Formula: Si3N4
Informal Name: silicon nitride
Structure Type: Polycrystalline
Manufacturer: ESK
Commercial Name: EKasin-D
Process: Hot Isostatic Pressing

Si3N4

Material number 2 of 8
in SCD Citation Number: Z00430
Fracture Toughness
Specimen
Size
( mm x mm )
Notch
Polishing
 
Fracture
Toughness
( MPa m1/2 )
3 x 4 hand 5.10 ± 0.09
2 x 2.5 machine 4.97 ± 0.12
Measurement Method: Unlisted
Evaluation Status: Evaluated by acceptance criteria

Material Specification and Properties for ZrO2

Material number 3 of 8
in SCD Citation Number: Z00430
Chemical Class: Oxide
Chemical Family: Zr-O
Formula: ZrO2
Informal Name: zirconia (TZP)
Structure Type: Polycrystalline
Manufacturer: Toyo Soda Manufacturing Co.
Process: Sintering

ZrO2

Material number 3 of 8
in SCD Citation Number: Z00430
Fracture Toughness
Specimen
Size
( mm x mm )
Notch
Polishing
 
Fracture
Toughness
( MPa m1/2 )
3 x 4 hand 5.48 ± 0.30
2 x 2.25 machine 4.69 ± 0.09
Measurement Method: Single-edge V-notched beam
Evaluation Status: Evaluated by acceptance criteria

Material Specification and Properties for Si3N4·xSiC

Material number 4 of 8
in SCD Citation Number: Z00430
Chemical Class: Nitride
Chemical Family: Si-N:SiC
Formula: Si3N4·xSiC
Informal Name: silicon nitride composite
Structure Type: Polycrystalline
Manufacturer: Japan Metals and Chemicals Co.
Process: Sintering

Si3N4·xSiC

Material number 4 of 8
in SCD Citation Number: Z00430
Fracture Toughness
Specimen
Size
( mm x mm )
Notch
Polishing
 
Fracture
Toughness
( MPa m1/2 )
3 x 4 hand 6.38 ± 0.10
3 x 4 hand 6.31 ± 0.04
2 x 2.5 machine 6.22 ± 0.10
Measurement Method: Single-edge V-notched beam
Evaluation Status: Evaluated by acceptance criteria

Material Specification and Properties for Al2O3

Material number 5 of 8
in SCD Citation Number: Z00430
Chemical Class: Oxide
Chemical Family: Al-O
Formula: Al2O3
Informal Name: alumina
Structure Type: Polycrystalline
Manufacturer: Desmarquest Co.
Commercial Name: AF997
Process: Sintering

Al2O3

Material number 5 of 8
in SCD Citation Number: Z00430
Fracture Toughness
Specimen
Size
( mm x mm )
Notch
Polishing
 
Fracture
Toughness
( MPa m1/2 )
2 x 2.5 machine 3.03 ± 0.11
Measurement Method: Single-edge V-notched beam
Evaluation Status: Evaluated by acceptance criteria

Material Specification and Properties for SiC

Material number 6 of 8
in SCD Citation Number: Z00430
Chemical Class: Carbide
Chemical Family: Si-C
Formula: SiC
Informal Name: silicon carbide
Structure Type: Polycrystalline
Manufacturer: Hutschenreuther
Process: Sintering

SiC

Material number 6 of 8
in SCD Citation Number: Z00430
Fracture Toughness
Specimen
Size
( mm x mm )
Notch
Polishing
 
Fracture
Toughness
( MPa m1/2 )
3 x 4 hand 5.07 ± 0.18
Measurement Method: Single-edge V-notched beam
Evaluation Status: Evaluated by acceptance criteria

Material Specification and Properties for Si3N4

Material number 7 of 8
in SCD Citation Number: Z00430
Chemical Class: Nitride
Chemical Family: Si-N
Formula: Si3N4
Informal Name: silicon nitride
Structure Type: Polycrystalline
Manufacturer: BASF
Process: Hot Pressing

Si3N4

Material number 7 of 8
in SCD Citation Number: Z00430
Fracture Toughness
Specimen
Size
( mm x mm )
Notch
Polishing
 
Fracture
Toughness
( MPa m1/2 )
3 x 4 hand 2.62 ± 0.10
Measurement Method: Single-edge V-notched beam
Evaluation Status: Evaluated by acceptance criteria

Material Specification and Properties for ZrO2·xMgO

Material number 8 of 8
in SCD Citation Number: Z00430
Chemical Class: Oxide
Chemical Family: Zr-O:MgO
Formula: ZrO2·xMgO
Informal Name: zirconia (PSZ)
Structure Type: Polycrystalline
Manufacturer: Friedrichsfeld Co.
Process: Sintering

ZrO2·xMgO

Material number 8 of 8
in SCD Citation Number: Z00430
Fracture Toughness
Specimen
Size
( mm x mm )
Notch
Polishing
 
Fracture
Toughness
( MPa m1/2 )
2 x 2.5 machine 7.08 ± 0.17
Measurement Method: Unlisted
Evaluation Status: Evaluated by acceptance criteria