NIST Structural Ceramics Database (SCD) Database

NIST Standard Reference Database 30

Last Update to Data Content: 2002

DOI: http://dx.doi.org/10.18434/T4F30D


SCD Citation Number: Z00594

Bibliographic Information

Reference:
"Elastic Constants and Crystal Anisotropy of Titanium Diboride," P.S. Spoor, J.D. Maynard, M.J. Pan, D.J. Green, J.R. Hellman, and T. Tanaka, Applied Physics Letters, Vol. 70 [15], pp. 1959-1961 (1997), published by American Institute of Physics.
Language: English

General Materials Processing Notes

The authors cite T. Tanaka et al., J. Phys. C, Vol. 13, 6671 (1980), and summarize the procedure as follows. "A cube of TiB2 single crystal, approximately 2 mm on each side, was used for the measurement. The single crystal was grown using a floating zone technique... No major impurities were detected in the single crystal using fluorescent x-ray analysis. ... The stoichiometry of the single crystal was determined to be TiB1.97."

Measurement Methods

Resonant ultrasound method
"The TiB2 crystal was oriented using the Laue method and then polished into the shape of a parallelepiped. It is held very lightly at two of its opposing corners between two piezoelectric film transducers... one is used as a drive transducer and the other as a receiver. As the drive frequency is swept, the output of the receiver shows peaks at the sample's natural resonances, and these can be compared to theoretical calculations of the normal modes of vibration of an elastic parallelepiped. Using elastic moduli as free parameters, a nonlinear least-squares fit to the resonant frequency data provides accurate estimates of the elastic moduli."

Index of Materials and Properties

Material Number 1: TiB2

Material Specification and Properties for TiB2

Material number 1 of 1
in SCD Citation Number: Z00594
Chemical Class: Boride
Chemical Family: Ti-B
Formula: TiB2
Informal Name: titanium diboride
Structure Type: Single Crystal
Manufacturer: In-House
Process: Floating zone

TiB2

Material number 1 of 1
in SCD Citation Number: Z00594
Elasticity Tensor
C(i,j)
Component
 
C(i,j)
Value
( GPa )
C(1,1) 660
C(1,2) 48
C(1,3) 93
C(3,3) 432
C(4,4) 260

Measurement Method: Resonant ultrasound method
Evaluation Status: Evaluated by acceptance criteria