NIST Standard Reference Database 30
Last Update to Data Content: 2002
"Elastic Constants and Crystal Anisotropy of Titanium Diboride," P.S. Spoor, J.D. Maynard, M.J. Pan, D.J. Green, J.R. Hellman, and T. Tanaka, Applied Physics Letters, Vol. 70 [15], pp. 1959-1961 (1997), published by American Institute of Physics.Language: English
The authors cite T. Tanaka et al., J. Phys. C, Vol. 13, 6671 (1980), and summarize the procedure as follows. "A cube of TiB2 single crystal, approximately 2 mm on each side, was used for the measurement. The single crystal was grown using a floating zone technique... No major impurities were detected in the single crystal using fluorescent x-ray analysis. ... The stoichiometry of the single crystal was determined to be TiB1.97."
"The TiB2 crystal was oriented using the Laue method and then polished into the shape of a parallelepiped. It is held very lightly at two of its opposing corners between two piezoelectric film transducers... one is used as a drive transducer and the other as a receiver. As the drive frequency is swept, the output of the receiver shows peaks at the sample's natural resonances, and these can be compared to theoretical calculations of the normal modes of vibration of an elastic parallelepiped. Using elastic moduli as free parameters, a nonlinear least-squares fit to the resonant frequency data provides accurate estimates of the elastic moduli."
| C(i,j) Component |
C(i,j) Value ( GPa ) |
|---|---|
| C(1,1) | 660 |
| C(1,2) | 48 |
| C(1,3) | 93 |
| C(3,3) | 432 |
| C(4,4) | 260 |