NIST Structural Ceramics Database (SCD) Database

NIST Standard Reference Database 30

Last Update to Data Content: 2002

DOI: http://dx.doi.org/10.18434/T4F30D


SCD Citation Number: Z00619

Bibliographic Information

Reference:
"Manufacturing and High Temperature Mechanical Properties of Si-N-O Ceramic Fibers," M. Sato and K. Okamura, Journal of the Ceramic Society of Japan, Vol. 106 [3], pp. 248-255 (1998), published by Ceramic Society of Japan.
Language: English

General Materials Processing Notes

"Synthesis of Si-N-O ceramic fibers: ... Polycarbosilane was melt-spun at 310 °C in an N2 gas by monohole method. The obtained polycarbosilane fibers had a diameter of 18 µm. The polycarbosilane fibers were thermal oxidation cured by the heat treatment in a temperature between 145 °C and 180 °C at the heating rate of 10 °C·h-1 in an O2 gas (purity: 99.99%). ... The curing was achieved at each temperature for 1 h. The cured polycarbosilane fibers were heated at the heating rate of 100 °C·h-1 from room temperature to 1200 °C, 1300 °C, 1400 °C, 1450 °C, and 1500 °C in a stream of NH3 gas (purity: 99.99%), and were kept for 1 h at each temperature so that Si-N-O ceramic fibers were obtained."

Measurement Methods

Tensile test
"Tensile strength and Young's modulus of Si-N-O ceramic fibers were measured by a universal testing machine made by Toyo Baldwin Co., Ltd., Tensilon UTM-II-20 (25 mm gage length and 2 mm·min-1 crosshead speed at room temperature)."

Index of Materials and Properties

Material Number 1: Si1.00N1.23O0.43

Material Specification and Properties for Si1.00N1.23O0.43

Material number 1 of 1
in SCD Citation Number: Z00619
Chemical Class: Oxynitride
Chemical Family: Si-N-O
Formula: Si1.00N1.23O0.43
Informal Name: silicon oxynitride
Structure Type: Polycrystalline
Manufacturer: In-House
Process: Pyrolysis

Si1.00N1.23O0.43

Material number 1 of 1
in SCD Citation Number: Z00619
Elastic Modulus
Fiber Cure
Temperature
( °C )
Processing
Temperature
( °C )
Elastic
Modulus
( GPa )
145 1200 67
145 1300 103
145 1400 113
155 1200 94
155 1300 138
155 1400 148
155 1450 156
155 1500 178
160 1200 103
160 1300 132
160 1400 143
160 1450 164
160 1500 185
165 1200 110
165 1300 114
165 1400 123
165 1450 134
165 1500 164
175 1200 81
175 1300 101
175 1400 107
175 1450 117
175 1500 122
180 1200 74
180 1300 109
180 1400 117
180 1450 124

Measurement Method: Tensile test
Evaluation Status: Evaluated by acceptance criteria
Cautions:
Specimens were Si-N-O ceramic fibers. Data were digitized from Fig. 7b of the reference.

Si1.00N1.23O0.43

Material number 1 of 1
in SCD Citation Number: Z00619
Tensile Strength
Fiber Cure
Temperature
( °C )
Processing
Temperature
( °C )
Tensile
Strength
( MPa )
145 1200 710
145 1300 1250
145 1400 800
145 1450 20
145 1500 10
155 1200 1270
155 1300 1510
155 1400 1520
155 1450 1440
155 1500 850
160 1200 1150
160 1300 1590
160 1400 1800
160 1450 1510
160 1500 1140
165 1200 1020
165 1300 1190
165 1400 1410
165 1450 1210
165 1500 1060
175 1200 880
175 1300 1300
175 1400 1030
175 1450 850
175 1500 470
180 1200 940
180 1300 1420
180 1400 930
180 1450 680
180 1500 20

Measurement Method: Tensile test
Evaluation Status: Evaluated by acceptance criteria
Cautions:
Specimens were Si-N-O ceramic fibers. Data were digitized from Fig. 7a of the reference.