NIST Standard Reference Database 30
Last Update to Data Content: 2002
"High-Temperature Creep of Yttria-Stabilized Zirconia Single Crystals," J. Martinez-Fernandez, M. Jimenez-Melendo, A. Dominguez-Rodriguez, and A.H. Heuer, Journal of the American Ceramic Society, Vol. 73 [8], pp. 2452-2456 (1990), published by American Ceramic Society.Language: English
"Single crystals of 9.4 mol% Y2O3 stabilized c-ZrO2, optically transparent and grown by skull melting, were used. Crystals were oriented by the Laue X-ray back-reflection technique and cut with a low-speed diamond saw into parallelepipeds, about 2.5 mm x 2.5 mm x 5.0 mm. The faces of the samples were mechanically polished with 8 µm, 5 µm, and 2 µm diamond pastes. The long axis (the loading axis) was parallel to [-1-12] while the other two faces were parallel to (111) and (1-10)."
The authors cite H. Gervais et al., Rev. Int. Hautes Temp. Refract., Vol. 15, 43 (1978), and summarize the procedure as follows. "Creep tests were performed in compression under constant load in a testing machine... Pads cut from the same crystals being deformed, but with a lower Schmid factor, were used to avoid indentation in and reaction between the polycrystalline Al2O3 rams and the specimens."
| Temperature Range ( °C ) | Creep Activatn Energy ( kJ mol-1 ) |
|---|---|
| 1300 - 1400 | 714 |
| 1450 - 1550 | 589 |
| Applied Stress ( MPa ) | Temperature ( °C ) | Creep Rate ( 10-9 s-1 ) |
|---|---|---|
| 100 | 1563 | 10000 |
| 100 | 1557 | 8400 |
| 100 | 1517 | 3700 |
| 100 | 1517 | 3100 |
| 100 | 1517 | 2800 |
| 100 | 1501 | 2800 |
| 100 | 1501 | 2300 |
| 100 | 1466 | 950 |
| 100 | 1457 | 1000 |
| 100 | 1451 | 720 |
| 100 | 1439 | 600 |
| 100 | 1436 | 460 |
| 100 | 1410 | 240 |
| 100 | 1410 | 200 |
| 100 | 1410 | 170 |
| 100 | 1399 | 190 |
| 100 | 1399 | 140 |
| 100 | 1390 | 140 |
| 100 | 1387 | 120 |
| 100 | 1390 | 98 |
| 100 | 1382 | 82 |
| 100 | 1382 | 68 |
| 100 | 1346 | 25 |
| 100 | 1346 | 23 |
| 100 | 1297 | 4.5 |
Data were digitized from Fig. 2 of the reference.
| Temperature Range ( °C ) | Creep Rate Exponent ( no unit ) |
|---|---|
| 1300 - 1400 | 7.3 ± 0.5 |
| 1450 - 1550 | 4.5 ± 0.4 |