NIST Structural Ceramics Database (SCD) Database

NIST Standard Reference Database 30

Last Update to Data Content: 2002

DOI: http://dx.doi.org/10.18434/T4F30D


SCD Citation Number: Z00624

Bibliographic Information

Reference:
"High-Temperature Creep of Yttria-Stabilized Zirconia Single Crystals," J. Martinez-Fernandez, M. Jimenez-Melendo, A. Dominguez-Rodriguez, and A.H. Heuer, Journal of the American Ceramic Society, Vol. 73 [8], pp. 2452-2456 (1990), published by American Ceramic Society.
Language: English

General Materials Processing Notes

"Single crystals of 9.4 mol% Y2O3 stabilized c-ZrO2, optically transparent and grown by skull melting, were used. Crystals were oriented by the Laue X-ray back-reflection technique and cut with a low-speed diamond saw into parallelepipeds, about 2.5 mm x 2.5 mm x 5.0 mm. The faces of the samples were mechanically polished with 8 µm, 5 µm, and 2 µm diamond pastes. The long axis (the loading axis) was parallel to [-1-12] while the other two faces were parallel to (111) and (1-10)."

Measurement Methods

Creep test (compression)
The authors cite H. Gervais et al., Rev. Int. Hautes Temp. Refract., Vol. 15, 43 (1978), and summarize the procedure as follows. "Creep tests were performed in compression under constant load in a testing machine... Pads cut from the same crystals being deformed, but with a lower Schmid factor, were used to avoid indentation in and reaction between the polycrystalline Al2O3 rams and the specimens."

Index of Materials and Properties

Material Number 1: ZrO2·xY2O3

Material Specification and Properties for ZrO2·xY2O3

Material number 1 of 1
in SCD Citation Number: Z00624
Chemical Class: Oxide
Chemical Family: Zr-O:Y2O3
Formula: ZrO2·xY2O3
Informal Name: zirconia (cubic)
Structure Type: Single Crystal
Manufacturer: In-House
Process: Melt Processing

ZrO2·xY2O3

Material number 1 of 1
in SCD Citation Number: Z00624
Creep Activation Energy
Temperature
Range
( °C )
Creep Activatn
Energy
( kJ mol-1 )
1300 - 1400 714
1450 - 1550 589

Measurement Method: Creep test (compression)
Evaluation Status: Evaluated by acceptance criteria

ZrO2·xY2O3

Material number 1 of 1
in SCD Citation Number: Z00624
Creep Rate
Applied
Stress
( MPa )
Temperature
 
( °C )
Creep Rate
 
( 10-9 s-1 )
100 1563 10000
100 1557 8400
100 1517 3700
100 1517 3100
100 1517 2800
100 1501 2800
100 1501 2300
100 1466 950
100 1457 1000
100 1451 720
100 1439 600
100 1436 460
100 1410 240
100 1410 200
100 1410 170
100 1399 190
100 1399 140
100 1390 140
100 1387 120
100 1390 98
100 1382 82
100 1382 68
100 1346 25
100 1346 23
100 1297 4.5

Measurement Method: Creep test (compression)
Evaluation Status: Evaluated by acceptance criteria
Cautions:
Data were digitized from Fig. 2 of the reference.

ZrO2·xY2O3

Material number 1 of 1
in SCD Citation Number: Z00624
Creep Rate Exponent
Temperature
Range
( °C )
Creep Rate
Exponent
( no unit )
1300 - 1400 7.3 ± 0.5
1450 - 1550 4.5 ± 0.4

Measurement Method: Creep test (compression)
Evaluation Status: Evaluated by acceptance criteria