NIST Standard Reference Database 30
Last Update to Data Content: 2002
"X-ray Studies on Highly Pure Magnesium Oxide," R.A. Brown, Nature, Vol. 208, pp. 481-481 (1965), published by Macmillan Magazines Ltd..Language: English
The author cites R.A. Brown, Amer. Ceram. Soc. Bull., Vol. 44, No. 6, 483 (1965), and summarize the procedure as follows. "High-purity (99.999 per cent) magnesium oxide was prepared by the thermal decomposition of pure magnesium oxalate dihydrate."
"Prior to the X-ray examination, the magnesium oxide was recrystallized by firing as a pressed disk at 1500 °C for 14 h. X-ray powder diffraction data were obtained by means of a 19 cm diameter camera using copper Kα-radiation with a nickel filter, and standard procedures."
| Axis | Axis Length ( Å ) |
|---|---|
| a | 4.2119(5) |
Cubic cell (fcc) with z = 4