NIST Structural Ceramics Database (SCD) Database

NIST Standard Reference Database 30

Last Update to Data Content: 2002

DOI: http://dx.doi.org/10.18434/T4F30D


SCD Citation Number: Z00638

Bibliographic Information

Reference:
"Microwave Plasma Sintering of Nanocrystalline Alumina," J. Peng, P. Hong, S. Dai, D. Vollath, and D.V. Szabo, Journal of Materials Science and Technology, Vol. 14, pp. 173-175 (1998), published by Allerton Press, Inc..
Language: English

General Materials Processing Notes

"The nanocrystalline alumina powders were produced by microwave plasma... The reaction was performed in a 50 mm diameter vessel made of quartz, passing a TE01 mode cavity in succession connected to a 0.915 GHz microwave generator. ... The nanocrystalline alumina powders were pressed at 400 MPa into 0.8 cm diameter discs. The single mode (TE113) tunable cylindrical resonant cavity with 2.45 GHz was used as the microwave plasma sintering apparatus."

Measurement Methods

Vickers indentation
"Microhardness was measured on polished surface by the Vickers microhardness tester (Fischerscope H100, Helmut Fischer Ltd. Germany), using loads of 100 mN for 20 s. Typical standard deviation was ±6 GPa for Vickers microhardness. Generally not less than ten different regions were sampled to obtain the average hardness of each specimen."

Index of Materials and Properties

Material Number 1: Al2O3

Material Specification and Properties for Al2O3

Material number 1 of 1
in SCD Citation Number: Z00638
Chemical Class: Oxide
Chemical Family: Al-O
Formula: Al2O3
Informal Name: alumina
Structure Type: Polycrystalline
Manufacturer: In-House
Process: Sintering

Al2O3

Material number 1 of 1
in SCD Citation Number: Z00638
Hardness
Powder Grain
Size Range
( nm )
Relative
Density
( % )
Hardness
 
( GPa )
4-8 78.3 12.1
4-8 89.6 20.8
4-8 99.2 28.4
50-100 69.9 5.0
50-100 79.8 11.4
50-100 88.7 16.3

Measurement Method: Vickers indentation
Evaluation Status: Evaluated by acceptance criteria
Cautions:
Data were digitized from Fig. 3 of the reference.