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NIST X-ray Photoelectron Spectroscopy Database (SRD 20), Version 5.0

Details Summary:
Summary Page
Tab Page Summary

General:
Element:
Ni
Formula:
(Ni(OH)2)0.75(H2O)0.16(NiCO3)0.09
Name:
nickel(II) hydroxide carbonate hydrate
CAS Registry No:
Class:
hydroxide

Citation:
Author Name(s):
Mansour A.N., Melendres C.A.
Journal:
Surf. Sci. Spectra 3, 247
DOI:
Pub Year:
1994

Data Processing:
Data Type:
Photoelectron Line
Line Designation:
2p3/2
Binding Energy (eV)
855.80
Energy Uncertainty:
Background Subtraction Method:
Shirley
Peak Location Method:
mixed Gaussian/Lorentzian
Full Width at Half-maximum Intensity (eV):
2.48
Gaussian Width (eV):
Lorentzian Width (eV):

Measurement:
Use of X-ray Monochromator:
No
Anode Material:
Mg
X-ray Energy:
Overall Energy Resolution (eV):
Calibration:
Cu 3p3, 2p3 = 75.13, 932.67
Charge Reference:
Adventitious carbon
Energy Scale Evaluation:
Reliable, with two-point correction of energy scale
Comment:
The composition was determined by thermogravimetry. The composition determined by XPS was Ni37.2O50.9C11.9. FAT mode. Emission angle = 45 degrees. The relative intensity of the Ni2p3/2 component was 0.65.

Specimen:
Specimen:
Method of Determining Specimen Composition:
X-ray Photoelectron Spectroscopy
Method of Determining Specimen Crystallinity:
Specimen Temperature (K):
300
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