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NIST X-ray Photoelectron Spectroscopy Database (SRD 20), Version 5.0

Details Summary:
Summary Page
Tab Page Summary

General:
Element:
Tc
Formula:
TcCl[(C4H7N2O)2(C4H6N2O)(C4H9BO3)]
XPS Formula:
Tc*Cl[(C4H7N2O)2(C4H6N2O)(C4H9BO3)]
Name:
chloro-tris(2,3-butanedione dioxime)-n-butylboronate technetium(III)
CAS Registry No:
104716-20-3
Class:
butanedione dioximato, chloride, nitrogen, organometallic

Citation:
Author Name(s):
Thompson M., Nunn A.D., Treher E.
Journal:
Anal. Chem. 58, 3100
DOI:
Pub Year:
1986

Data Processing:
Data Type:
Photoelectron Line
Line Designation:
3d5/2
Binding Energy (eV)
255.40
Energy Uncertainty:
0.2
Background Subtraction Method:
Peak Location Method:
data
Full Width at Half-maximum Intensity (eV):
Gaussian Width (eV):
Lorentzian Width (eV):

Measurement:
Use of X-ray Monochromator:
Yes
Anode Material:
Mg
X-ray Energy:
Overall Energy Resolution (eV):
Calibration:
Charge Reference:
Internal hydrocarbon
Energy Scale Evaluation:
Reliable, with one-point correction of energy scale
Comment:
dmg= dimethylglyoxime; bub = n-butyl boronic acid; A gold mask and an electron flood gun (Ep =10 eV) were used to control sample charging.

Specimen:
Specimen:
Method of Determining Specimen Composition:
Method of Determining Specimen Crystallinity:
Specimen Temperature (K):
300
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