NIST X-ray Photoelectron Spectroscopy Database

NIST X-ray Photoelectron Spectroscopy Database (SRD 20), Version 5.0

Details Summary:

Tab Page Summary

General:

Tc

(NH₄)₂TcBr₆

(NH₄)₂Tc*Br₆

diammonium technetium(IV) hexabromide

CAS Registry No:

75493-13-9

ammonium, bromide

Citation:

Author Name(s):

Thompson M., Nunn A.D., Treher E.

Anal. Chem. 58, 3100

Pub Year:

1986

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Total Records: 47

Element

Atomic No

Formula

Spectral Line

Energy (eV)

Details

Tc

43

NH₄TcO₄

3d_5/2

259.30

N

7

NH₄TcO₄

1s

401.90

O

8

NH₄TcO₄

1s

531.60

Tc

43

[(CH₃)₄N]₂TcCl₆

3d_5/2

257.40

Cl

17

[(CH₃)₄N]₂TcCl₆

2p_3/2

198.20

N

7

[(CH₃)₄N]₂TcCl₆

1s

402.90

Br

35

TcBr[(C₄H₇N₂O)₂(C₄H₆N₂O)(C₄H₉BO₃)]

3d_5/2

68.20

N

7

TcBr[(C₄H₇N₂O)₂(C₄H₆N₂O)(C₄H₉BO₃)]

1s

400.50

O

8

TcBr[(C₄H₇N₂O)₂(C₄H₆N₂O)(C₄H₉BO₃)]

1s

532.40

B

5

TcBr[(C₄H₇N₂O)₂(C₄H₆N₂O)(C₄H₉BO₃)]

1s

190.70

Tc

43

TcBr[(C₄H₇N₂O)₂(C₄H₆N₂O)(C₄H₉BO₃)]

3d_5/2

255.40

Cl

17

TcCl[(C₄H₇N₂O)₂(C₄H₆N₂O)(C₄H₉BO₃)]

2p_3/2

197.60

N

7

TcCl[(C₄H₇N₂O)₂(C₄H₆N₂O)(C₄H₉BO₃)]

1s

400.60

O

8

TcCl[(C₄H₇N₂O)₂(C₄H₆N₂O)(C₄H₉BO₃)]

1s

532.90

B

5

TcCl[(C₄H₇N₂O)₂(C₄H₆N₂O)(C₄H₉BO₃)]

1s

190.50

Tc

43

TcCl[(C₄H₇N₂O)₂(C₄H₆N₂O)(C₄H₉BO₃)]

3d_5/2

255.40

O

8

TcCl[(C₆H₉N₂O)₂(C₆H₈N₂O)(CH₃BO₃)]

1s

532.30

B

5

TcCl[(C₆H₉N₂O)₂(C₆H₈N₂O)(CH₃BO₃)]

1s

190.90

Tc

43

TcCl[(C₆H₉N₂O)₂(C₆H₈N₂O)(CH₃BO₃)]

3d_5/2

255.50

Cl

17

TcCl[(C₆H₉N₂O)₂(C₆H₈N₂O)(CH₃BO₃)]

2p_3/2

197.60

N

7

TcCl[(C₆H₉N₂O)₂(C₆H₈N₂O)(CH₃BO₃)]

1s

400.60

Tc

43

(NH₄)₂TcBr₆

3d_5/2

256.60

Br

35

(NH₄)₂TcBr₆

3d_5/2

68.40

N

7

(NH₄)₂TcBr₆

1s

402.60

Br

35

[Tc((CH₃)₂PCH₂CH₂P(CH₃)₂)₂Br₂]Br

3d_5/2

66.70

Br

35

[Tc((CH₃)₂PCH₂CH₂P(CH₃)₂)₂Br₂]Br

3d_5/2

68.60

P

15

[Tc((CH₃)₂PCH₂CH₂P(CH₃)₂)₂Br₂]Br

2p_3/2

130.80

Tc

43

[Tc((CH₃)₂PCH₂CH₂P(CH₃)₂)₂Br₂]Br

3d_5/2

255.10

Tc

43

[Tc((CH₃)₂AsC₆H₄As(CH₃)₂)₂Br₂]Br

3d_5/2

255.40

Br

35

[Tc((CH₃)₂AsC₆H₄As(CH₃)₂)₂Br₂]Br

3d_5/2

67.00

Data Processing:

Photoelectron Line

Line Designation:

3d_5/2

Binding Energy (eV)

256.60

Energy Uncertainty:

0.2

Background Subtraction Method:

Peak Location Method:

data

Full Width at Half-maximum Intensity (eV):

Gaussian Width (eV):

Lorentzian Width (eV):

Measurement:

Use of X-ray Monochromator:

Yes

Anode Material:

Mg

X-ray Energy:

Overall Energy Resolution (eV):

Calibration:

Charge Reference:

Adventitious carbon

Energy Scale Evaluation:

Reliable, with one-point correction of energy scale

Comment:

A gold mask and electron flood gun at a setting of 10 eV were used to control sample charging.

Specimen:

Method of Determining Specimen Composition:

Method of Determining Specimen Crystallinity:

Specimen Temperature (K):

300

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