NIST X-ray Photoelectron Spectroscopy Database

NIST X-ray Photoelectron Spectroscopy Database (SRD 20), Version 5.0

Details Summary:

Tab Page Summary

General:

Element:

Formula:

[Tc((CH₃)₂PCH₂CH₂P(CH₃)₂)₂Cl₂]Cl

XPS Formula:

[Tc((CH₃)₂PCH₂CH₂P(CH₃)₂)₂Cl₂]Cl*

Name:

dichloro di(1,2-bis(dimethylphosphine)ethane) technetium(III) chloride

CAS Registry No:

80537-73-1

Class:

chloride, organometallic

Citation:

Author Name(s):

Thompson M., Nunn A.D., Treher E.

Journal:

Anal. Chem. 58, 3100

DOI:

Pub Year:

1986

bookAll Records in this Publication

Data Processing:

Photoelectron Line

2p_3/2

196.60

0.2

Background Subtraction Method:

Peak Location Method:

data

Full Width at Half-maximum Intensity (eV):

Gaussian Width (eV):

Lorentzian Width (eV):

Measurement:

Use of X-ray Monochromator:

Yes

Anode Material:

X-ray Energy:

Overall Energy Resolution (eV):

Calibration:

Charge Reference:

Internal hydrocarbon

Energy Scale Evaluation:

Reliable, with one-point correction of energy scale

Comment:

[Tc(dmpe)2Cl2]Cl, dmpe=bis(dimethylphosphine)ethane. A gold mask and electron flood gun at a setting of 10 eV were used to control sample charging.

Specimen:

Method of Determining Specimen Composition:

Method of Determining Specimen Crystallinity:

Specimen Temperature (K):

300