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NIST X-ray Photoelectron Spectroscopy Database (SRD 20), Version 5.0

Details Summary:
Summary Page
Tab Page Summary

General:
Element:
N
Formula:
Zr[Cr3.0O2.5(OH)3.6](C4H5N)1.9Cu0.8(PO4)2.0.9H2O
XPS Formula:
neutral nitrogen
Name:
zirconium phosphate hydrate - chromium oxyde hydrate - copper(II) - pyrrole (Zr[Cr3.0O2.5(OH)3.6](C4H5N)1.9Cu0.8(PO4)2.0.9H2O)
CAS Registry No:
Class:
addition compound, hydrate, other ring, phosphate, pyrrole

Citation:
Author Name(s):
Maireles-Torres P., Olivera-Pastor P., Castellon E.R., Lopez A.J.
Journal:
J. Inclusion Phenom. Mol. Recogn. Chem. 14, 327
DOI:
Pub Year:
1992

Data Processing:
Data Type:
Photoelectron Line
Line Designation:
1s
Binding Energy (eV)
399.10
Energy Uncertainty:
0.2
Background Subtraction Method:
Peak Location Method:
data
Full Width at Half-maximum Intensity (eV):
Gaussian Width (eV):
Lorentzian Width (eV):

Measurement:
Use of X-ray Monochromator:
No
Anode Material:
Al
X-ray Energy:
Overall Energy Resolution (eV):
Calibration:
Charge Reference:
Internal hydrocarbon
Energy Scale Evaluation:
Reliable, with one-point correction of energy scale
Comment:
The sample was prepared by the reaction of gaseous pyrrole with Cu2+ exchanged chromia-pillared alpha-zirconium phosphate and calcined (T = 673 K). The composition was determined using chemical, thermal and CNH analyses. The intensity ratio of the neutral/charged nitrogen components was 5.72.

Specimen:
Specimen:
Method of Determining Specimen Composition:
Method of Determining Specimen Crystallinity:
X-ray Diffraction
Specimen Temperature (K):
300
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