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NIST X-ray Photoelectron Spectroscopy Database (SRD 20), Version 5.0

Details Summary:
Summary Page
Tab Page Summary

General:
Element:
Ni
Formula:
Cs4(B11H11)2Ni
Name:
tetracesium bis(undecahydroundecaborato)nickelate
CAS Registry No:
Class:
alkali, borane/caborane, nickelate

Citation:
Author Name(s):
Kester J.G., Keller D., Huffman J.C., Benefiel M.A., Geiger W.E., Jr, Atwood C. et al.
Journal:
Inorg. Chem. 33, 5438
DOI:
Pub Year:
1994

Data Processing:
Data Type:
Photoelectron Line
Line Designation:
2p3/2
Binding Energy (eV)
854.80
Energy Uncertainty:
Background Subtraction Method:
Peak Location Method:
data
Full Width at Half-maximum Intensity (eV):
Gaussian Width (eV):
Lorentzian Width (eV):

Measurement:
Use of X-ray Monochromator:
Yes
Anode Material:
Al
X-ray Energy:
Overall Energy Resolution (eV):
Calibration:
Ni2p3 = 852.73
Charge Reference:
Adventitious carbon
Energy Scale Evaluation:
Reliable, with one-point correction of energy scale
Comment:
The sample was heated to 353 K before analysis. An electron flood gun (Ep = 2 eV, Ip = 0.4 mA) was used for charge compensation.

Specimen:
Specimen:
Method of Determining Specimen Composition:
Method of Determining Specimen Crystallinity:
X-ray Diffraction
Specimen Temperature (K):
300
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