NIST X-ray Photoelectron Spectroscopy Database

NIST X-ray Photoelectron Spectroscopy Database (SRD 20), Version 5.0

Details Summary:

One Page Summary

Instruction: Click on selected Tab for more information.

Element:

Formula:

[Tc((C₆H₅)₂PCH₂CH₂P(C₆H₅)₂)₂Cl₂]Cl

XPS Formula:

[Tc*((C₆H₅)₂PCH₂CH₂P(C₆H₅)₂)₂Cl₂]Cl

Name:

dichloro di(1,2-bis(diphenylphosphine)ethane) technetium(III) chloride

CAS Registry No:

91467-32-2

Class:

chloride, organometallic, phenyl benzene

Author Name(s):

Thompson M., Nunn A.D., Treher E.

Journal:

Anal. Chem. 58, 3100

DOI:

Pub Year:

1986

book All Records in this Publication

Photoelectron Line

3d_5/2

255.50

0.2

Background Subtraction Method:

Peak Location Method:

data

Full Width at Half-maximum Intensity (eV):

Gaussian Width (eV):

Lorentzian Width (eV):

Use of X-ray Monochromator:

Yes

Anode Material:

X-ray Energy:

Overall Energy Resolution (eV):

Calibration:

Charge Reference:

Internal hydrocarbon

Energy Scale Evaluation:

Reliable, with one-point correction of energy scale

Comment:

[Tc(dppe)2Cl2]Cl, dppe=bis(diphenylphosphine)ethane. A gold mask and an electron flood gun (Ep =10 eV) were used to control sample charging.

Specimen:

powder (when a special point is made in the article)

Method of Determining Specimen Composition:

Method of Determining Specimen Crystallinity:

Specimen Temperature (K):

300