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NIST X-ray Photoelectron Spectroscopy Database (SRD 20), Version 5.0

Details Summary:
Summary Page
Tab Page Summary

General:
Element:
C
Formula:
CH3OD/Pd
XPS Formula:
adsorbed methanol and methoxy
Name:
methanol/palladium(CH3OD/Pd)
CAS Registry No:
67-56-1
Class:
alcohol, catalyst, oxygen

Citation:
Author Name(s):
Rebholz M., Kruse N.
Journal:
J. Chem. Phys. 95, 7745
DOI:
Pub Year:
1991

Data Processing:
Data Type:
Photoelectron Line
Line Designation:
1s
Binding Energy (eV)
286.07
Energy Uncertainty:
Background Subtraction Method:
other
Peak Location Method:
Gaussian
Full Width at Half-maximum Intensity (eV):
1.2
Gaussian Width (eV):
Lorentzian Width (eV):

Measurement:
Use of X-ray Monochromator:
Yes
Anode Material:
Al
X-ray Energy:
Overall Energy Resolution (eV):
Calibration:
Au4f7,Pd3d5 = 84.00,335.12
Charge Reference:
Conductor
Energy Scale Evaluation:
Reliable, with one-point correction of energy scale
Comment:
1.4 L CH3OD were adsorbed onto Pd(111)-(1x1) at 90 K. The substrate was cleaned by cycles of Ar+ ion bombardment (Ep = 600 - 1000 eV, j = 2 microampres cm-2, T = 1050 K), annealing (T = 1200 K) and O2 treatment (p = 1E-5 Pa, T = 1000 K).

Specimen:
Specimen:
Method of Determining Specimen Composition:
X-ray Photoelectron Spectroscopy
Method of Determining Specimen Crystallinity:
Low-energy Electron Diffraction
Specimen Temperature (K):
90
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