Overall Energy Resolution (eV):
Calibration:
Au = 84.00, Cr2p3 = 574.35
Charge Reference:
Conductor
Energy Scale Evaluation:
Reliable, with two-point correction of energy scale
Comment:
Oxidation of Ni foil in air at 573 K for 24 h, following by heating in vacuo at 373 K for 1 h to remove surface hydration. The O1s/Ni3p atom ratio for this film is 1.4.
metal foil, oxidizing atmosphere, oxygen pressure
Method of Determining Specimen Composition:
X-ray Photoelectron Spectroscopy
Method of Determining Specimen Crystallinity:
Specimen Temperature (K):
300