NIST X-ray Photoelectron Spectroscopy Database

NIST X-ray Photoelectron Spectroscopy Database (SRD 20), Version 5.0

Details Summary:

Tab Page Summary

General:

Element:

Formula:

TcCl[(C₆H₉N₂O)₂(C₆H₈N₂O)(CH₃BO₃)]

XPS Formula:

TcCl*[(C₆H₉N₂O)₂(C₆H₈N₂O)(CH₃BO₃)]

Name:

chloro-tris(cyclohexane-1,2-dione dioxime)-methylboronate technetium(III)

CAS Registry No:

104716-22-5

Class:

chloride, organometallic, other ring

Citation:

Author Name(s):

Thompson M., Nunn A.D., Treher E.

Journal:

Anal. Chem. 58, 3100

DOI:

Pub Year:

1986

bookAll Records in this Publication

Data Processing:

Photoelectron Line

2p_3/2

197.60

0.2

Background Subtraction Method:

Peak Location Method:

data

Full Width at Half-maximum Intensity (eV):

Gaussian Width (eV):

Lorentzian Width (eV):

Measurement:

Use of X-ray Monochromator:

Yes

Anode Material:

X-ray Energy:

Overall Energy Resolution (eV):

Calibration:

Charge Reference:

Internal hydrocarbon

Energy Scale Evaluation:

Reliable, with one-point correction of energy scale

Comment:

cdo=cyclohexyldioxime; mb= methylboronic acid. A gold mask and electron flood gun at a setting of 10 eV were used to control sample charging.

Specimen:

Method of Determining Specimen Composition:

Method of Determining Specimen Crystallinity:

Specimen Temperature (K):

300