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NIST X-ray Photoelectron Spectroscopy Database (SRD 20), Version 5.0

Details Summary:
Summary Page
Tab Page Summary

General:
Element:
O
Formula:
((-CH2C(CH3)(C(O)OC4H9)-)3(-CH2C(CH3)(C(O)OC(CH3)3)-)7)n
XPS Formula:
Ether oxygen atoms
Name:
n-butyl methacrylate - t-butyl methacrylate copolymer (3:7)
CAS Registry No:
Class:
ester, nitrogen, oxygen, polymer, sulfur

Citation:
Author Name(s):
Castner D.G., Ratner B.D.
Journal:
Surf. Interface Anal. 15, 479
DOI:
Pub Year:
1990

Data Processing:
Data Type:
Photoelectron Line
Line Designation:
1s
Binding Energy (eV)
533.10
Energy Uncertainty:
Background Subtraction Method:
other
Peak Location Method:
Gaussian
Full Width at Half-maximum Intensity (eV):
Gaussian Width (eV):
Lorentzian Width (eV):

Measurement:
Use of X-ray Monochromator:
Yes
Anode Material:
Al
X-ray Energy:
Overall Energy Resolution (eV):
Calibration:
Charge Reference:
Internal hydrocarbon
Energy Scale Evaluation:
Reliable, with one-point correction of energy scale
Comment:
The copolymer was synthesized from monomers dissolved in toluene using azobis(isobutyronitrile as a catalyst. An electron flood gun (Ep = 5 eV) was used for charge compensation. The spectra were recorded at normal emission. The C/O intensity ratio was 81

Specimen:
Specimen:
Method of Determining Specimen Composition:
Method of Determining Specimen Crystallinity:
Specimen Temperature (K):
293
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