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NIST X-ray Photoelectron Spectroscopy Database (SRD 20), Version 5.0

Details Summary:
Summary Page
Tab Page Summary

General:
Element:
Pb
Formula:
Pb2Ru2O7-x
XPS Formula:
Pb(IV) state
Name:
lead ruthenium oxides
CAS Registry No:
Class:
catalyst, double oxide, non-stoichiometric oxide, oxide

Citation:
Author Name(s):
Gokagac G., Kennedy B.J.
Journal:
J. Electroanal. Chem. 353, 71
DOI:
Pub Year:
1993

Data Processing:
Data Type:
Photoelectron Line
Line Designation:
4f7/2
Binding Energy (eV)
138.10
Energy Uncertainty:
Background Subtraction Method:
other
Peak Location Method:
Gaussian
Full Width at Half-maximum Intensity (eV):
Gaussian Width (eV):
Lorentzian Width (eV):

Measurement:
Use of X-ray Monochromator:
No
Anode Material:
Mg
X-ray Energy:
Overall Energy Resolution (eV):
Calibration:
Charge Reference:
Adventitious carbon
Energy Scale Evaluation:
Reliable, with one-point correction of energy scale
Comment:
The sample was prepared by solid state reaction of stoichiometric quantities of an intimate mixture of PbO and RuO2 pressed in pellets (T = 853 K, time = 15 h, T = 923 K, time = 15 h and T = 1023 K, time = 50 h) with regrinding after each heating step. FAT mode. Lead+ruthenium pyrochlore

Specimen:
Specimen:
Method of Determining Specimen Composition:
Method of Determining Specimen Crystallinity:
X-ray Diffraction
Specimen Temperature (K):
300
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