Comment:
The sample was prepared by solid state reaction of stoichiometric quantities of an intimate mixture of PbO and RuO2 pressed in pellets (T = 853 K, time = 15 h, T = 923 K, time = 15 h and T = 1023 K, time = 50 h) with regrinding after each heating step. FAT mode. Lead+ruthenium pyrochlore