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IUPAC-NIST Solubility Database
NIST Standard Reference Database 106
Solubility System:
1,1,1-Trichloroethane with Water.
Components:
(1) 1,1,1-Trichloroethane; C2H3Cl3; [71-55-6]
NIST Chemistry WebBook
for detail
(2) Water; H2O; [7732-18-5]
NIST Chemistry WebBook
for detail
Original Measurements:
Lees, F.P.; Sarram, P., J. Chem. Eng. Data 1971, 16, 41-4.
Variables:
Temperature = 298 K
Prepared By:
A. L. Horvath
Experimental Data:
(Notes on the Nomenclature)
t/°C
10
2
* Mass Fraction w
1
10
3
* Mole Fraction x
1
(compiler)
10
2
* w
1
/M
1
(compiler) [mol g**-1]
25
5.0 x 10
-2
3.69
2.8 x 10
-3
Method/Apparatus/Procedure:
The apparatus containing the organic-water system was held in a waterbath thermostat. The stirring of the mixture was effected by a glass rod rotated by a horseshoe magnet for about 48 hours. The concentration of water in the organic phase was determined by the Karl Fischer titration method.
Source and Purity of Materials:
(1) Distilled.
(2) Source not given. Analytical grade, degassed and used without further purification.
Estimated Errors:
Solubility: ± 2 %.
Temperature: ± 0.1 K.