IUPAC-NIST Solubility Database
NIST Standard Reference Database 106

Glass Ball as Bullet Solubility System: 1,2,4-Tribromobenzene with Water
Components:
   (1) 1,2,4-Tribromobenzene; C6H3Br3; [615-54-3]  NIST Chemistry WebBook for detail
   (2) Water; H2O; [7732-18-5]  NIST Chemistry WebBook for detail
Original Measurements:
   Yalkowsky, S.H.; Orr, R.J.; Valvani, S.C., Ind. Eng. Chem. Fundam. 1979, 18(4), 351-3.

 Variables:
   Temperature = One temperature

 Prepared By:
   A. Vesala

 Experimental Data:   (Notes on the Nomenclature)
  
t/°C102 * g1/V2 [g dm**-3]105 * Concentration c1 [mol dm**-3]Concent. c1 Note107 * Mole Fraction x1x1 Note
251.013.2b5.78a
 Notes:
   a  Calculated by F. W. Getzen.
   b  Reported.

 Method/Apparatus/Procedure:
   A small excess of solute in water was agitated for a period of 4-48 hours (the exact time for equilibration was not reported in single cases) and then filtered. The saturated solution was extracted with a small volume of methylene chloride which was then assayed spectrophotometrically. At least two independent determinations were carried out.

 Source and Purity of Materials:
   (1) Commercial reagent (Aldrich or Eastman), used as received.
   (2) Source and purity not specified.

 Estimated Errors:
   Solubility: ± 10% (authors).
   Temperature: ± 1 K (authors).