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IUPAC-NIST Solubility Database
NIST Standard Reference Database 106
Solubility System:
1,2-Dichlorobenzene with Water
Components:
(1) Water; H2O; [7732-18-5]
NIST Chemistry WebBook
for detail
(2) 1,2-Dichlorobenzene; C6H4Cl2; [95-50-1]
NIST Chemistry WebBook
for detail
Original Measurements:
Goldman, S., Ph.D. Dissertation, McGill University, Montreal, 1969, p 84.
Variables:
Temperature = Temperature
Prepared By:
A. L. Horvath
Experimental Data:
(Notes on the Nomenclature)
t/°C
10
1
* g
1
/V
2
[g dm**-3]
10
2
* Concentration c
1
[mol dm**-3]
Concent. c
1
Note
10
3
* Mole Fraction x
1
x
1
Note
25
4.342
2.41
b
2.719
c
35.1
5.783
3.21
b
3.650
c
45.06
7.909
4.39
b
5.028
c
Notes:
a
Calculated by F. W. Getzen.
b
Reported.
c
Calculated by compiler.
Method/Apparatus/Procedure:
Equilibrium experiments were carried out in a constant temperature water bath using a stirrer. An equilibration period of at least 5 days was allowed. The total water content in the organic phase was determined by a Karl Fischer titration. Each reported water solubility was obtained as an average of at least two independent determinations.
Source and Purity of Materials:
(1) Distilled.
(2)Reagent grade, washed with conc. H
2
SO
4
and with 1 M NaHCO
3
and then fractionally distilled over silica gel.
Estimated Errors:
Solubility: ±4%.
Temperature: ±0.1 K.