IUPAC-NIST Solubility Database
NIST Standard Reference Database 106


Glass Ball as Bullet Solubility System: 1,3-Dichlorobenzene with Water

Components:
   (1) Water; H2O; [7732-18-5]  NIST Chemistry WebBook for detail
   (2) 1,3-Dichlorobenzene; C6H4Cl2; [541-73-1]  NIST Chemistry WebBook for detail

Original Measurements:
   Klemenc, A.; Low, M., Rec. Trav. Chim. Pays-Bas 1930, 49(4), 629-40.

Variables:
   Temperature = Temperature

Prepared By:
   A. L. Horvath

Experimental Data:   (Notes on the Nomenclature)
  
t/°C103 * Molality mol1/kgmol1/kg Note101 * g1/kgg1/kg Note105 * Mole Fraction x1x1 Note
200.7550b1.11a1.360c
250.8366b1.23a1.507c
300.9522b1.40a1.716c
351.020b1.50a1.838c
401.136b1.67a2.047c
451.204b1.77a2.169c
551.333b1.96a2.402c
601.367b2.01a2.463c
Notes:
   a  Reported.
   b  Calculated by F. W. Getzen.
   c  Calculated by compiler.

Method/Apparatus/Procedure:
   The determinations of the solubility was based upon volumetric principles applied to the measurement of excess solute in a calibrated apparatus as described by Rex (1).

Source and Purity of Materials:
   (1) Kahlbaum reagent, purified by the method of Friedel and Crafts before use.
   (2) Distilled.

Estimated Errors:
   Solubility: ±10% (compiler).
   Temperature: ± 1 K. (compiler).

References:
   1Rex, A. Z. Phys. Chem. 1906, 55(A), 355-70.