IUPAC-NIST Solubility Database
NIST Standard Reference Database 106


Glass Ball as Bullet Solubility System: Pentane with Water

Components:
   (1) Water; H2O; [7732-18-5]  NIST Chemistry WebBook for detail
   (2) Pentane; C5H12; [109-66-0]  NIST Chemistry WebBook for detail

Original Measurements:
   Connolly, J.F., J. Chem. Eng. Data 1966, 11, 13-6.

Variables:
   Temperature = 300-325 °C
   Pressure = 150-700 atm

Prepared By:
   M.C. Haulait-Pirson

Experimental Data:   (Notes on the Nomenclature)
  
Solubility of pentane in water
t/°CPressure [atm]Pressure (compiler) [MPa]g1/100 g solutionMole Fraction x1 (compiler)
30015015.21.30.0033
30018518.71.70.0043
30035035.41.70.0043
30060060.71.60.0040
30070070.91.50.0038
33017017.22.10.0053
33019519.73.30.0084
33022022.24.00.0103
33026026.34.60.0119
33035035.44.90.0127
33048549.14.70.0122
33067067.84.00.0103
34023023.35.20.0135
34025025.36.10.0160
34027527.86.90.0182
34033033.47.60.0201
3403503547.60.0201
34047047.66.90.0182
34062062.85.70.0149
35024024.317.80.0207
35022525.839.00.0241
35026526.8410.30.0279
35028028.3612.10.0332
35030030.3913.90.0387
35032532.9215.50.0438
35035035.4615.50.0438
35039540.0113.90.0387
35044545.0812.00.0329
35051051.6610.30.0279
35059059.779.00.0241
35228028.3615.80.0442
35228028.3618.40.0533
35228028.3621.00.0622
35228028.3623.30.0705
35240040.5240.70.1463
35239039.5138.70.1362
35238539.0036.50.1255
35238038.4934.00.1140
35237537.9931.40.1026
35237537.9928.50.0905
35237537.9928.40.0784
35237537.9923.30.0705
35238038.4921.00.0622
35239039.5118.40.0533
35242042.5515.70.0444
Method/Apparatus/Procedure:
   The cloud point method was used. Measurements were carried out in a 100 mL stainless-steel cell. The cell was loaded with 15 g (2) and brought to temperature. Mixing was started and (1) was injected, until either a cloud or a small portion of a second phase appeared at the top of the cell. Then mercury was injected to change the pressure, more (1) was injected and the preocedure was repeated.

Source and Purity of Materials:
   (1) Phillips reagent grade; better than 99.8% used as received.
   (2) distilled and deaerated.

Estimated Errors:
   Solubility: ± 2 atm (accuracy)
   Temperature: ± 0.02 K