IUPAC-NIST Solubility Database
NIST Standard Reference Database 106


Glass Ball as Bullet Solubility System: Ethene with Water

Components:
   (1) Ethene; C2H4; [74-85-1]  NIST Chemistry WebBook for detail
   (2) Water; H2O; [7732-18-5]  NIST Chemistry WebBook for detail

Original Measurements:
   Sanchez, M.; Lentz, H., High Temp. - High Press. 1973, 5, 689-699.

Variables:
   Temperature = 439.15 K to 573.15 K
   Pressure = 10.0 to 94.5 MPa

Prepared By:
   W. Hayduk

Experimental Remarks:

   Smoothed values as obtained by extrapolation and interpolation are also available in this paper.

Experimental Data:   (Subscripts 1,2,3, ..., in column headings refer to components 1,2,3, ...)
  
t/°CT/KTemp NotePressure [bar]Pressure [MPa]Pressure NotePressure (compiler) [MPa]Mole Fraction (x1)x1 NoteMole Fraction of Gas (y1)y1 Note
166439.15 (1)11001018.600.004in Liquid0.860in Gas
166439.15 (1)115015113.350.005in Liquid0.890in Gas
166439.15 (1)163563.5160.900.010in Liquid0.959in Gas
166439.15194594.5186.00(0.008)10.910in Gas
250523.15 (1)119019.0111.970.014in Liquid0.630in Gas
250523.15 (1)124024.0116.510.018in Liquid0.688in Gas
250523.15 (1)137537.5128.730.026in Liquid0.766in Gas
250523.15 (1)157057.0142.750.034in Liquid0.750in Gas
250523.15 (1)173073.0159.130.040in Liquid0.810in Gas
300573.15 (1)124024.0112.380.024in Liquid0.516in Gas
300573.15 (1)138038.0122.690.036in Liquid0.597in Gas
300573.15 (1)155055.0130.250.047in Liquid0.550in Gas
Notes:
   1  Calculated by compiler.
   2  Brackets as in original paper.

Method/Apparatus/Procedure:
   The apparatus consisted of a high pressure piston pump, Bourdon pressure gauges, a stainless steel capillary tube equilibrium cell 4.7 mm in inside diameter, a tubular storage chamber for the gas, as well as an associated temperature sensing element, sampling probes and valves. The apparatus was mounted in a constant temperature chamber. The equilibrium cell was charged with a known quantity of solvent by rotating it to a horizontal position. The quantity of gas was determined by material balance and the PV relation in the gas supply tube.

Source and Purity of Materials:
   1. Ethene purity was specified to be 99.99%.
   2. Water was double distilled.

Estimated Errors:
   Solubility: δx1/x1 = ± 0.05 or ± 5% (Compiler)
   Temperature: δT/K = ± 0.5