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IUPAC-NIST Solubility Database
NIST Standard Reference Database 106
Solubility System:
Acenaphthene with 1-Propanol
Components:
(1) 1-Propanol; C3H8O; [71-23-8]
NIST Chemistry WebBook
for detail
(2) Acenaphthene; C12H10; [83-32-9]
NIST Chemistry WebBook
for detail
Original Measurements:
Speyers, C.L., Am. J. Sci. 1902, 14, 293-302.
Variables:
Temperature = Temperature
Prepared By:
W. E. Acree, Jr.
Experimental Data:
(Notes on the Nomenclature)
T/K
Mole Fraction x
1
Mole Fraction x
2
273.2
0.0088
0.9912
283.7
0.0097
0.9903
304.3
0.0188
0.9812
323.5
0.0437
0.9563
346.6
0.199
0.801
Method/Apparatus/Procedure:
Experimental procedure only marginally described by author. Excess solute and solvent were equilibrated in a constant temperature water bath for between 10-30 minutes. Saturated solution was withdrawn through a coarse filter and analyzed by specific gravity. Author noted that evaporation to dryness and weighing the residue was subject to too much decomposition.
Source and Purity of Materials:
(1) Purity not given, Kahlbaum, was recrystallized from alcohol to a melting point temperature of 93.5 °C.
(2) Purity not given, Kahlbaum, was dried over calcium oxide and distilled before use.
Estimated Errors:
Solubility:
x
1
: ± 8 % (relative error, compiler).
Temperature:
T
/K: precision ± 0.1.
References:
1
W.E. Acree, Jr.