IUPAC-NIST Solubility Database
NIST Standard Reference Database 106

Glass Ball as Bullet Solubility System: Phenanthrene with 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7-pentadecafluoroheptane
Components:
   (1) Phenanthrene; C14H10; [85-01-8]  NIST Chemistry WebBook for detail
   (2) 1,1,2,2,3,3,4,4,5,5,6,6,7,7-pentadecafluoroheptane; C7HF15; [375-83-7]  NIST Chemistry WebBook for detail
Original Measurements:
   McLaughlin, E.; Scott, R.L., J. Phys. Chem. 1956, 60, 674-676.

 Variables:
   Temperature = 298 K

 Prepared By:
   W.E. Acree, Jr.

 Experimental Data:   (Notes on the Nomenclature)
  
t/°CMole Fraction x1Mole Fraction x2
25.00.001600.9984
 Method/Apparatus/Procedure:
   Constant temperature bath, a precision thermometer and uv/visible spectrometer.
Mixtures of known concentrations sealed in glass ampoules and allowed to equilibrate at a constant temperature for an unspecified length of time. Solubilities calculated from spectral absorbance data at 270 nm.

 Source and Purity of Materials:
   (1) White Label, Eastman Kodak Company, Rochester, New York, USA, was recrystallized ten times from ethanol.
   (2) Purity not specified, synthesized by authors, was fractionally distilled shortly before use.

 Estimated Errors:

   Temperature: T/K: precision ± 0.01. x1: ± 3 % (relative error; compiler).