IUPAC-NIST Solubility Database
NIST Standard Reference Database 106


Glass Ball as Bullet Solubility System: Carbon dioxide with Sodium chloride and Water

Components:
   (1) Sodium chloride; NaCl; [7647-14-5]  NIST Chemistry WebBook for detail
   (2) Carbon dioxide; CO2; [124-38-9]  NIST Chemistry WebBook for detail
   (3) Water; H2O; [7732-18-5]  NIST Chemistry WebBook for detail

Original Measurements:
   He, S.; Morse, J.W., Geochim. Cosmochim. Acta 1993, 57, 3533-54.

Variables:
   Temperature = 273.15 K to 363.15 K
   Pressure = 0.1032 MPa
   Concentration = m2/mol kg-1 = 0.1 - 6.14

Prepared By:
   Pirketta Scharlin

Experimental Data:   (Subscripts 1,2,3, ..., in column headings refer to components 1,2,3, ...)
  
T/KTemp Note102 * Pressure [atm]Pressure NoteDensity ρ [g/cm3]Density Note103 * Molality m1 [mol/kg]m1 NoteMolality m2 [mol/kg]m2 Noteγγ Note
273.15a96.6d1.0214c63.6e0.5b1.18f
273.15a96.6d1.0411c57.8e1.0b1.30f
273.15a96.6d1.0787c45.7e2.0b1.65f
273.15a96.6d1.1140c39.5e3.0b1.90f
273.15a96.6d1.1460c31.7e4.0b2.38f
273.15a96.6d1.1776c26.9e5.0b2.79f
273.15a96.6d1.2095c21.9e6.0b3.44f
298.15a3.9d1.0189c1.20e0.5b1.10f
298.15a3.9d1.0363c1.10e1.0b1.18f
298.15a3.9d1.0700c0.90e2.0b1.48f
298.15a3.9d1.1026c0.80e3.0b1.76f
298.15a3.9d1.1340c0.60e4.0b2.25f
298.15a3.9d1.1642c0.50e5.0b2.61f
298.15a3.9d1.1974c0.40e6.14b3.21f
323.15a85.4d1.0081c15.5e0.5b1.07f
323.15a85.4d1.0262c14.7e1.0b1.13f
323.15a85.4d1.0608c13.3e2.0b1.25f
323.15a85.4d1.0934c10.6e3.0b1.56f
323.15a85.4d1.1240c9.2e4.0b1.81f
323.15a85.4d1.1524c8.4e5.0b1.98f
323.15a85.4d1.1824c7.4e6.14b2.25f
348.15a60.3d0.9795c7.8e0.1b1.03f
348.15a60.3d1.0120c7.4e1.0b1.09f
348.15a60.3d1.0463c7.0e2.0b1.15f
348.15a60.3d1.1090c6.4e4.0b1.26f
348.15a60.3d1.1638c5.9e6.0b1.37f
363.15a30.1d0.9624c3.4e0.1b1.02f
363.15a30.1d1.0028c3.2e1.0b1.06f
363.15a30.1d1.0373c3.1e2.0b1.12f
363.15a30.1d1.1002c2.8e4.0b1.21f
363.15a30.1d1.1559c2.6e6.0b1.30f
Notes:
   a  Calculated by the compiler.
   b  m2 = molality of NaCl
   c  ρ = density of solvent
   d  P1 = partial pressure of CO2
   e  m1 = molality of CO2
   f  γ1 = activity coefficient of CO2

Method/Apparatus/Procedure:
   Either pure CO2 gas or CO2-N2 mixtures were used in the experiments to maintain a constant P(CO2). The CO2-N2 mixtures were made by pumping predetermined amounts of CO2 and N2 into a gas tank and their composition was verified by gas chromatography.
CO2 or CO2-N2 gas mixtures were equilibrated with the aqueous solutions in a series of stirred water-jacketed reaction vessels with condensers. The gas was premoistured by first passing it through distilled water at the temperature of experiment. Fine bubbles were obtained by using gas-dispersion tubes. The bubbling rate was 90- 95 mL min-1.
The mole fraction of CO2 in the CO2-N2 mixture was determined using a Hewlett Packard (5790A) gas chromatograph.

Source and Purity of Materials:
   (1) Commercial; purity 99.9 %
   (2) Source not mentioned. Analytical reagent-grade which met ACS specifications.
Vacuum-dried before use.
   (3) 18 MΩ water obtained from a Milli-Q Super-Q water system.

Estimated Errors:
   Solubility: δm1/m1 = ± 0.012
δγ11 = ± 0.04
   Temperature: δT/K = ± 0.1