IUPAC-NIST Solubility Database
NIST Standard Reference Database 106

Glass Ball as Bullet Solubility System: 1,1,2,2-Tetrachloroethane with Water.

   (1) Water; H2O; [7732-18-5]  NIST Chemistry WebBook for detail
   (2) 1,1,2,2-Tetrachloroethane; C2H2Cl4; [79-34-5]  NIST Chemistry WebBook for detail

Original Measurements:
   Schwarz, F.P., Anal. Chem. 1980, 52, 10-15.

   Temperature = 297 K

Prepared By:
   A. L. Horvath

Experimental Data:   (Notes on the Nomenclature)
t/°C102 * Mass Fraction w1104 * Mole Fraction x1 (compiler)102 * w1/M1 (compiler) [mol g**-1]
23.50.2963.181.76 x 10-3
   The aqueous solubility was determined by elution chromatography. The solute columns (3 mm o.d., 2 mm i.d., and 40 cm long) were filled with Chromosorb P. The analysis consisted of removing a segment of the column packing and placing it into a  test tube containing n-octane. Then, samples were injected into a gas chromatograph for analysis. The average deviations were calculated from several measurements on different samples.

Source and Purity of Materials:
   (1) Commercial reagent of spectral grade, used as received.
   (2) Distilled.

Estimated Errors:
   Solubility: ± 3.0 % std. dev.
   Temperature: ± 1.5 K.