IUPAC-NIST Solubility Database
NIST Standard Reference Database 106

Glass Ball as Bullet Solubility System: 1,1,2,2-Tetrachloroethane with Water.
Components:
   (1) Water; H2O; [7732-18-5]  NIST Chemistry WebBook for detail
   (2) 1,1,2,2-Tetrachloroethane; C2H2Cl4; [79-34-5]  NIST Chemistry WebBook for detail
Original Measurements:
   Schwarz, F.P.; Miller, J., Anal. Chem. 1980, 52(13), 2162-4.

 Variables:
   Temperature = 283 K - 303 K

 Prepared By:
   A. L. Horvath

 Experimental Data:   (Notes on the Nomenclature)
  
t/°C102 * Mass Fraction w1104 * Mole Fraction x1 (compiler)102 * w1/M1 (compiler) [mol g**-1]
10.00.372+/-0.0074.012.22 x 10-3
20.00.385+/-0.0174.152.19 x 10-3
30.00.367+/-0.0073.952.19 x 10-3
 Method/Apparatus/Procedure:
   The aqueous solubility was determined by elution chromatography. The solute columns (3 mm o.d., 1.8 mm i.d.) were positioned vertically in a waterbath thermostat. The measurement time interval ranged from 1 day to 2 weeks. The average deviations  were calculated from several measurements on different samples. The elution chromatography method has been described elsewhere.1

 Source and Purity of Materials:
   (1) Commercial reagent grade, used as received.
   (2) Distilled.

 Estimated Errors:
   Solubility: 4 %.
   Temperature: ± 0.5 K.

 References:
   1F. P. Schwarz, Anal. Chem. 52, 10 (1980).