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IUPAC-NIST Solubility Database
NIST Standard Reference Database 106
Solubility System:
1,1,2,2-Tetrachloroethane with Water.
Components:
(1) Water; H2O; [7732-18-5]
NIST Chemistry WebBook
for detail
(2) 1,1,2,2-Tetrachloroethane; C2H2Cl4; [79-34-5]
NIST Chemistry WebBook
for detail
Original Measurements:
Vogel, A.I., rev. by Furniss, B.S., et al. Vogel's Textbook of Practical Organic Chemistry, 5th ed. (Longman, London, 1989), p. 1442.
Variables:
Temperature = 293 K
Prepared By:
A. L. Horvath
Experimental Data:
(Notes on the Nomenclature)
t/°C
10
2
* Mass Fraction w
1
10
4
* Mole Fraction x
1
(compiler)
10
2
* w
1
/M
1
(compiler) [mol g**-1]
20.0
0.29
3.12
1.73 x 10
-3
Method/Apparatus/Procedure:
The solubility determination was carried out in small test tubes (e. g. 100 × 12 mm) to permit vigorous shaking of the solvent and solute mixtures. During the experiment, 0.20 cm
3
1,1,2,2-tetrachloroethane was added to 3.0 cm
3
of water and agitated concentration of 1,1,2,2-tetrachloroethane in water was analyzed by passing the sample through a chromatographic column.
Source and Purity of Materials:
(1) Commercial reagent, used as received.
(2) Distilled.
Estimated Errors:
Solubility: Not specified.
Temperature: ± 1 K (compiler).