IUPAC-NIST Solubility Database
NIST Standard Reference Database 106

Glass Ball as Bullet Solubility System: 1,1,2,2-Tetrachloroethane with Water.

   (1) Water; H2O; [7732-18-5]  NIST Chemistry WebBook for detail
   (2) 1,1,2,2-Tetrachloroethane; C2H2Cl4; [79-34-5]  NIST Chemistry WebBook for detail

Original Measurements:
   Vogel, A.I., rev. by Furniss, B.S., et al. Vogel's Textbook of Practical Organic Chemistry, 5th ed. (Longman, London, 1989), p. 1442.

   Temperature = 293 K

Prepared By:
   A. L. Horvath

Experimental Data:   (Notes on the Nomenclature)
t/°C102 * Mass Fraction w1104 * Mole Fraction x1 (compiler)102 * w1/M1 (compiler) [mol g**-1] x 10-3
   The solubility determination was carried out in small test tubes (e. g. 100 × 12 mm) to permit vigorous shaking of the solvent and solute mixtures. During the experiment, 0.20 cm3 1,1,2,2-tetrachloroethane was added to  3.0 cm3 of water and agitated concentration of 1,1,2,2-tetrachloroethane in water was analyzed by passing the sample through a chromatographic column.

Source and Purity of Materials:
   (1) Commercial reagent, used as received.
   (2) Distilled.

Estimated Errors:
   Solubility: Not specified.
   Temperature: ± 1 K (compiler).