IUPAC-NIST Solubility Database
NIST Standard Reference Database 106

Glass Ball as Bullet Solubility System: 1,1,1-Trichloroethane with Water.
Components:
   (1) 1,1,1-Trichloroethane; C2H3Cl3; [71-55-6]  NIST Chemistry WebBook for detail
   (2) Water; H2O; [7732-18-5]  NIST Chemistry WebBook for detail
Original Measurements:
   Orlandini, M.; Fermeglia, M.; Kikic, I.; Alessi, P., Chem. Eng. J. 1983, 26, 245-50.

 Variables:
   Temperature = 293 K

 Prepared By:
   A. L. Horvath

 Experimental Data:   (Notes on the Nomenclature)
  
t/°C102 * Mass Fraction w1 (compiler) 102 * Mass Fraction w2 (compiler)104 * Mole Fraction x1103 * Mole Fraction x2
200.1332.90 x 10-21.82.14
 Method/Apparatus/Procedure:
   A mixture of 1,1,1-trichloroethane and water was agitated overnight and left at equilibrium for 24 hours. Three samples were withdrawn for each phase with a syringe and analyzed by gas chromatography. The gas chromatograph (C. Erba ATc/t) was  equipped with a Shimadzu Chromatopac E-1A integrator. A stainless column packed with 100-120 mesh Chromosorb W DMCD coated with heptadecane nitrile was used for analysis.

 Source and Purity of Materials:
   (1) Fluka reagent, purified by distillation before use.
   (2) Distilled (compiler).

 Estimated Errors:
   Solubility: Not specified.
   Temperature: ± 0.1 K.