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IUPAC-NIST Solubility Database
NIST Standard Reference Database 106
Solubility System:
Water with 1,1-Dichloroethane.
Components:
(1) 1,1-Dichloroethane; C2H4Cl2; [75-34-3]
NIST Chemistry WebBook
for detail
(2) Water; H2O; [7732-18-5]
NIST Chemistry WebBook
for detail
Original Measurements:
Staverman, A.J., Recl. Trav. Chim. Pays-Bas 1941, 60, 836-41.
Variables:
Temperature = 273 K - 303 K
Prepared By:
A. L. Horvath
Experimental Data:
(Notes on the Nomenclature)
t/°C
10
2
* Mass Fraction w
1
10
3
* Mole Fraction x
1
(compiler)
10
2
* w
1
/M
1
(compiler) [mol g**-1]
0
4.60 x 10
-2
2.54
2.55 x 10
-3
25
9.66 x 10
-2
5.31
5.36 x 10
-3
30
1.145 x 10
-1
6.30
6.36 x 10
-3
Method/Apparatus/Procedure:
Water was shaken with 1,1-dichloroethane for about 12 hours in a paraffin liquid bath thermostat. The water content of the organic phase was determined by the Karl Fischer titration method. All measurements were carried out in duplicate. The result is an average of two measurements. A full description of the method used is given in a thesis.
1
Source and Purity of Materials:
(1) Distilled.
(2) Source and purity not given.
Estimated Errors:
Solubility: Not specified.
Temperature: ± 0.5 K (compiler).
References:
1
A. J. Staverman, Ph. D. thesis, University of Leiden, Leiden, Belgium, 1938.