IUPAC-NIST Solubility Database
NIST Standard Reference Database 106

Glass Ball as Bullet Solubility System: 1,1-Dichloroethane with Water.
Components:
   (1) 1,1-Dichloroethane; C2H4Cl2; [75-34-3]  NIST Chemistry WebBook for detail
   (2) Water; H2O; [7732-18-5]  NIST Chemistry WebBook for detail
Original Measurements:
   McNally, M.E.; Grob, R.L., J. Chromatogr. 1983, 260, 23-32.

 Variables:
   Temperature = 303 K

 Prepared By:
   A. L. Horvath

 Experimental Data:   (Notes on the Nomenclature)
  
t/°C106 * g1/g2102 * Mass Fraction w1 (compiler) 104 * Mole Fraction x1 (compiler)
304.8344 x 1030.48118.793
 Method/Apparatus/Procedure:
   Standard solutions were prepared in 100 cm3 flask. They were shaken for 5 minutes and then allowed to equilibrate in a constant temperature bath held at 30 °C for 24 hours. Samples were pipetted in  headspace vials, sealed, thermostated and then examined by the gas chromatographic head space analysis technique. An F & M model 402 gas chromatograph, equipped with dual columns and dual flame ionization detectors, was used.

 Source and Purity of Materials:
   (1) Chemical Service, West Chester, PA., USA. Purest grade available.
   (2) Distilled and run through two Barnstead purification cartridges.

 Estimated Errors:
   Solubility: 3.13 % R. E.
   Temperature: ± 0.5 K (compiler).