IUPAC-NIST Solubility Database
NIST Standard Reference Database 106

Glass Ball as Bullet Solubility System: 1,1-Dichloroethane with Magnesium sulfate and Water.
Components:
   (1) 1,1-Dichloroethane; C2H4Cl2; [75-34-3]  NIST Chemistry WebBook for detail
   (2) Water; H2O; [7732-18-5]  NIST Chemistry WebBook for detail
   (3) Magnesium sulfate; MgSO4; [7487-38-9]  NIST Chemistry WebBook for detail
Original Measurements:
   Gross, P.M., Z. Phys. Chem. 1929, 6B, 215-20.

 Variables:
   Temperature = 298 K

 Prepared By:
   A. L. Horvath

 Experimental Data:   (Notes on the Nomenclature)
  
t/°C102 * g1/g210-3 * Concentration c2 [mol dm**-3]102 * Mass Fraction w1 (compiler) 104 * Mole Fraction x1 (compiler)
250.3160.50.3156.06
 Method/Apparatus/Procedure:
   A mixture of 10 to 20 cm3 1,1-dichloroethane in 500 cm3 of an aqueous MgSO4 solution in a bottle was placed in a water thermostat bath. The sample container was placed on a shaker and agitated until no more  liquid droplets remained undissolved. One or more samples were syphoned out and the concen-tration of the 1,1-dichloroethane was determined using a Zeiss water interferometer.

 Source and Purity of Materials:
   (1) Commercial reagent, fractionally distilled before use.
   (2) Kahlbaun chemical, certified grade.
   (3) Distilled.

 Estimated Errors:
   Solubility: ± 2 %.
   Temperature: ± 0.01 K.