IUPAC-NIST Solubility Database
NIST Standard Reference Database 106

Glass Ball as Bullet Solubility System: 2,3-Dichloro-1,3-butadiene with Water
Components:
   (1) Water; H2O; [7732-18-5]  NIST Chemistry WebBook for detail
   (2) 2,3-Dichloro-1,3-butadiene; C4H4Cl2; [1653-19-6]  NIST Chemistry WebBook for detail
Original Measurements:
   Vojtko, J.; Hrusovsky, M.; Kanala, A., Chemicke Zvesti, 21, 443 (1967)

 Variables:
   Temperature = 293 K

 Prepared By:
   A. L. Horvath

 Experimental Data:   (Notes on the Nomenclature)
  
t/°C102 * Mass Fraction w1102 * Mass Fraction w2105 * Mole Fraction x1 (compiler)102 * Mole Fraction x2 (compiler)
20>0.020.02>3.013.6
 Method/Apparatus/Procedure:
   The titration method as described elsewhere1 was used. Solubility data for the ternary system of water-methanol-2,3-dichloro-1,3-butadiene were also reported.

 Source and Purity of Materials:
   (1) Synthesis was described elsewhere.2 At 20°C, nD =1.4887 and d4 = 1.1838 g/cm3.
   (2) Distilled.

 Estimated Errors:
   Solubility: Not specified.
   Temperature: ± 1.0 K (compiler).

 References:
   1 D. F. Othmer, R. E. White, and E. Trueger, Ind. Eng. Chem. 33, 1240 (1941).
   2 W. H. Carothers and G. J. Berchett, J. Am. Chem. Soc. 55, 2004 (1933).