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IUPAC-NIST Solubility Database
NIST Standard Reference Database 106
Solubility System:
1,2,3-Trichloropropane with Water
Components:
(1) Water; H2O; [7732-18-5]
NIST Chemistry WebBook
for detail
(2) 1,2,3-Trichloropropane; C3H5Cl3; [96-18-4]
NIST Chemistry WebBook
for detail
Original Measurements:
Hutchinson, T.C.; Hellebust, J.A.; Tam, D., et al. Hydrocarbons and Halogenated Hydrocarbons in the Aquatic Environment, Plenum Press, New York, 1980, p. 577-86.
Variables:
Temperature = 298 K
Prepared By:
A. L. Horvath
Experimental Data:
(Notes on the Nomenclature)
t/°C
Density ρ [kg m**-3]
10
2
* Mass Fraction w
1
(compiler)
10
4
* Mole Fraction x
1
(compiler)
25
1.900
0.1906
2.33
Method/Apparatus/Procedure:
An excess quantity of 1,2,3-trichloropropane was added to water and stirred vigorously for 24 hrs. After settling at 25°C for 48 hours, the solution was extracted with cyclohexane. The samples were analyzed using an Aminco- Bowman spectrophotofluorometer. A detailed description of the method has been reported elsewhere.
1
Source and Purity of Materials:
(1) Aldrich Chemicals, highest grade available. Used as received.
(2) Double distilled.
Estimated Errors:
Solubility: Not specified.
Temperature: ± 0.2 K (compiler).
References:
1
D. Mackay and W. -Y. Shiu, J. Chem. Eng. Data 22, 399 (1977).